PMID- 10492703
OWN - NLM
STAT- MEDLINE
DCOM- 19991012
LR  - 20061115
IS  - 0265-203X (Print)
IS  - 0265-203X (Linking)
VI  - 16
IP  - 3
DP  - 1999 Mar
TI  - Solid phase microextraction of pesticide residues from strawberries.
PG  - 111-7
AB  - A new solid phase microextraction method for the determination of pesticide 
      residues in strawberries for 16 commonly used compounds was described. The 
      strawberries were crushed and centrifuged. An aliquot of the well agitated 
      aqueous supernatant (4 ml) was extracted with a fibre coated with 
      polydimethylsiloxane (PDMS, 100 microns) for 45 min at room temperature. 
      Identification and quantification were achieved using a gas chromatography-mass 
      spectrometry (GC-MS) system and selective ion monitoring (SIM). The method was 
      tested for the following pesticides: carbofuran, diethofencarb, penconazole, 
      hexaconazole, metalaxyl, folpet, bromopropylate, dichlofluanid, alpha-endosulfan, 
      beta-endosulfan, parathion ethyl, procymidone, iprodione, vinclozolin, 
      myclobutanil and chlorothalonil. Limits of detection, repeatability and linearity 
      for standard calibration in strawberries were obtained. Positive and negative 
      effects of the matrix between the extracting solution of strawberries and water 
      were observed. Stabilities of these compounds in the extracting solution of 
      strawberries were determined. The solvent-free SPME procedure was found to be 
      quicker and more cost effective than the solvent extraction methods commonly 
      used.
FAU - Hu, R
AU  - Hu R
AD  - Laboratoire de Physico et Toxico Chimie des Systemes Naturels, Equipe 
      Perigourdine de Chimie Appliquee (LPTCSN-EPCA), Perigueux, France.
FAU - Hennion, B
AU  - Hennion B
FAU - Urruty, L
AU  - Urruty L
FAU - Montury, M
AU  - Montury M
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
PL  - England
TA  - Food Addit Contam
JT  - Food additives and contaminants
JID - 8500474
RN  - 0 (Pesticide Residues)
SB  - IM
MH  - Calibration
MH  - *Food Contamination
MH  - Fruit/*chemistry
MH  - Gas Chromatography-Mass Spectrometry/methods
MH  - Humans
MH  - Pesticide Residues/*isolation & purification
MH  - Reproducibility of Results
EDAT- 1999/09/24 00:00
MHDA- 1999/09/24 00:01
CRDT- 1999/09/24 00:00
PHST- 1999/09/24 00:00 [pubmed]
PHST- 1999/09/24 00:01 [medline]
PHST- 1999/09/24 00:00 [entrez]
AID - 10.1080/026520399284154 [doi]
PST - ppublish
SO  - Food Addit Contam. 1999 Mar;16(3):111-7. doi: 10.1080/026520399284154.