PMID- 11227475
OWN - NLM
STAT- MEDLINE
DCOM- 20010322
LR  - 20191025
IS  - 0937-0633 (Print)
IS  - 0937-0633 (Linking)
VI  - 367
IP  - 5
DP  - 2000 Jul
TI  - Determination of palladium in airborne particulate matter in a German city.
PG  - 450-3
AB  - The part of palladium in ambient urban air that is bound to particles and soluble 
      in aqua regia was determined by means of sorbent extraction, coupled with 
      graphite furnace atomic absorption spectrometry (GFAAS) and laser absorption 
      fluorescence spectrometry (LAFS). Samples of about 200 m3 air were taken in a 
      suburb of Berlin, Germany. The coupling of the selective and automated 
      pre-concentration procedure for Pd as N,N-diethyl-N'-benzoylthiourea complex with 
      the respective detection methods proved to be sufficiently sensitive. Severe 
      interference with other matrix constituents, occurring mainly by direct LAFS 
      detection, could be overcome and the detection limit was improved tremendously. 
      The concentration of Pd in ambient air was determined to be in the range from 0.2 
      to 14.6 pg/m3.
FAU - Tilch, J
AU  - Tilch J
AD  - Institut fur Spektrochemie und angewandte Spektroskopie, Institutsteil Berlin, 
      Germany.
FAU - Schuster, M
AU  - Schuster M
FAU - Schwarzer, M
AU  - Schwarzer M
LA  - eng
PT  - Journal Article
PL  - Germany
TA  - Fresenius J Anal Chem
JT  - Fresenius' journal of analytical chemistry
JID - 9114077
RN  - 0 (Air Pollutants)
RN  - 0 (Dust)
RN  - 0 (Solutions)
RN  - 5TWQ1V240M (Palladium)
SB  - IM
MH  - Air Pollutants/*analysis
MH  - Dust/analysis
MH  - Equipment Design
MH  - Germany
MH  - Palladium/*analysis
MH  - Sensitivity and Specificity
MH  - Solutions
MH  - Spectrometry, Fluorescence/instrumentation/methods/standards
MH  - Spectrophotometry, Atomic/instrumentation/methods/standards
MH  - Urbanization
EDAT- 2001/03/03 10:00
MHDA- 2001/03/27 10:01
CRDT- 2001/03/03 10:00
PHST- 2001/03/03 10:00 [pubmed]
PHST- 2001/03/27 10:01 [medline]
PHST- 2001/03/03 10:00 [entrez]
AID - 10.1007/s002160000380 [doi]
PST - ppublish
SO  - Fresenius J Anal Chem. 2000 Jul;367(5):450-3. doi: 10.1007/s002160000380.