PMID- 12711203
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20030729
LR  - 20190901
IS  - 0379-0738 (Print)
IS  - 0379-0738 (Linking)
VI  - 132
IP  - 3
DP  - 2003 Apr 8
TI  - Optimization of extraction parameters for the chemical profiling of 
      3,4-methylenedioxymethamphetamine (MDMA) tablets.
PG  - 182-94
AB  - The extraction of impurities from illegally produced 
      3,4-methylenedioxymethamphetamine (MDMA) has been studied in order to optimize 
      the parameters. Two different MDMA samples were used. Particular attention was 
      paid to the influence of the pH, the evaporation step, and the sample storage. 
      The method used was an extraction of impurities by diethyl ether from a buffer 
      solution at pH 11.5, followed by gas chromatography (GC) mass spectrometric (MS) 
      analyses after a dryness concentration under monitored conditions of the ethereal 
      extract. Repeat extractions of the same sample gave an average relative standard 
      deviation (RSD) of less than 8.5% within day and less than 10.5% between days.
FAU - Gimeno, Pascal
AU  - Gimeno P
AD  - Laboratoire de Police Scientifique de Lyon, 31 Avenue Franklin Roosevelt, 69134, 
      Ecully, France.
FAU - Besacier, Fabrice
AU  - Besacier F
FAU - Chaudron-Thozet, Huguette
AU  - Chaudron-Thozet H
LA  - eng
PT  - Journal Article
PL  - Ireland
TA  - Forensic Sci Int
JT  - Forensic science international
JID - 7902034
EDAT- 2003/04/25 05:00
MHDA- 2003/04/25 05:01
CRDT- 2003/04/25 05:00
PHST- 2003/04/25 05:00 [pubmed]
PHST- 2003/04/25 05:01 [medline]
PHST- 2003/04/25 05:00 [entrez]
AID - S0379073803000197 [pii]
AID - 10.1016/s0379-0738(03)00019-7 [doi]
PST - ppublish
SO  - Forensic Sci Int. 2003 Apr 8;132(3):182-94. doi: 10.1016/s0379-0738(03)00019-7.