PMID- 12723928
OWN - NLM
STAT- MEDLINE
DCOM- 20030714
LR  - 20190729
IS  - 1060-3271 (Print)
IS  - 1060-3271 (Linking)
VI  - 86
IP  - 2
DP  - 2003 Mar-Apr
TI  - Determination of metals in composite diet samples by inductively coupled 
      plasma-mass spectrometry.
PG  - 439-47
AB  - A study was conducted to evaluate the applicability of inductively coupled 
      plasma-mass spectrometry (ICP-MS) techniques for determination of metals in 
      composite diets. Aluminum, cadmium, chromium, copper, lead, manganese, nickel, 
      vanadium, and zinc were determined by this method. Atmospheric pressure microwave 
      digestion was used to solubilize analytes in homogenized composite diet samples, 
      and this procedure was followed by ICP-MS analysis. Recovery of certified 
      elements from standard reference materials ranged from 92 to 119% with relative 
      standard deviations (RSDs) of 0.4-1.9%. Recovery of elements from fortified 
      composite diet samples ranged from 75 to 129% with RSDs of 0-11.3%. Limits of 
      detection ranged from 1 to 1700 ng/g; high values were due to significant amounts 
      of certain elements naturally present in composite diets. Results of this study 
      demonstrate that low-resolution quadrupole-based ICP-MS provides precise and 
      accurate measurements of the elements tested in composite diet samples.
FAU - Melnyk, Lisa Jo
AU  - Melnyk LJ
AD  - U.S. Environmental Protection Agency, 26 W. Martin Luther King Dr, Cincinnati, OH 
      45268, USA. melnyk.lisa@epa.gov
FAU - Morgan, Jeffrey N
AU  - Morgan JN
FAU - Fernando, Reshan
AU  - Fernando R
FAU - Pellizzari, Edo D
AU  - Pellizzari ED
FAU - Akinbo, Olujide
AU  - Akinbo O
LA  - eng
PT  - Journal Article
PT  - Research Support, U.S. Gov't, Non-P.H.S.
PL  - England
TA  - J AOAC Int
JT  - Journal of AOAC International
JID - 9215446
RN  - 0 (Indicators and Reagents)
RN  - 0 (Metals)
SB  - IM
MH  - Animals
MH  - Beverages/analysis
MH  - Calibration
MH  - Cattle
MH  - *Food Analysis
MH  - Hydrolysis
MH  - Indicators and Reagents
MH  - Liver/chemistry
MH  - Mass Spectrometry
MH  - Metals/*analysis
MH  - Reference Standards
EDAT- 2003/05/02 05:00
MHDA- 2003/07/15 05:00
CRDT- 2003/05/02 05:00
PHST- 2003/05/02 05:00 [pubmed]
PHST- 2003/07/15 05:00 [medline]
PHST- 2003/05/02 05:00 [entrez]
PST - ppublish
SO  - J AOAC Int. 2003 Mar-Apr;86(2):439-47.