PMID- 12947732
OWN - NLM
STAT- MEDLINE
DCOM- 20040715
LR  - 20151119
IS  - 1672-173X (Print)
IS  - 1672-173X (Linking)
VI  - 34
IP  - 2
DP  - 2003 Apr
TI  - [Determination of zearalenone and its metabolites in grains by capillary 
      electrophoresis].
PG  - 333-6
AB  - OBJECTIVE: To establish a method for the determination of zearalenone and its 
      metabolites in grains by capillary electrophoresis. METHODS: The samples were 
      extracted with liquid-liquid partition and ultrasonic extraction, cleaned up with 
      C18 cartridges, then determined by micellar electrokinetic capillary 
      chromatography (MEKC). RESULTS: The limits of detection for Zearalenone (ZON), 
      alpha-Zearalenol (alpha-ZOL), beta-Zearalenol (beta-ZOL), Aflatoxin B1 (AFT B1) 
      and Ochratoxin A (Och A) were 0.0084, 0.081, 0.14, 0.0016 and 0.031 microgram/ml, 
      respectively. Recoveries of all compounds were in the range of 77.9%-103.1%. 
      Relative standard deviations (RSDs) were 0.63%-1.98%. CONCLUSION: This sensitive 
      and accurate method can be used in the determination of zearalenone and its 
      metabolites in grains.
FAU - Zeng, Hongyan
AU  - Zeng H
AD  - Department of Sanitary Technology, West China School of Pulic Health, Sichuan 
      University, Chengdu 610041, China.
FAU - Li, Yuanqian
AU  - Li Y
FAU - Jin, Jun
AU  - Jin J
FAU - Sun, Huiqin
AU  - Sun H
LA  - chi
PT  - English Abstract
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
PL  - China
TA  - Sichuan Da Xue Xue Bao Yi Xue Ban
JT  - Sichuan da xue xue bao. Yi xue ban = Journal of Sichuan University. Medical 
      science edition
JID - 101162609
RN  - 0 (Mycotoxins)
RN  - 0 (Ochratoxins)
RN  - 0 (zearalenol)
RN  - 1779SX6LUY (ochratoxin A)
RN  - 5W827M159J (Zearalenone)
RN  - 76LO2L2V39 (Zeranol)
RN  - 9N2N2Y55MH (Aflatoxin B1)
SB  - IM
MH  - Aflatoxin B1/analysis
MH  - Chromatography, Micellar Electrokinetic Capillary
MH  - Edible Grain/*microbiology
MH  - Electrophoresis, Capillary
MH  - Food Contamination/*analysis
MH  - Food Microbiology
MH  - Mycotoxins/analysis
MH  - Ochratoxins/analysis
MH  - Zearalenone/*analysis/*metabolism
MH  - Zeranol/*analogs & derivatives/*analysis
EDAT- 2003/09/02 05:00
MHDA- 2004/07/16 05:00
CRDT- 2003/09/02 05:00
PHST- 2003/09/02 05:00 [pubmed]
PHST- 2004/07/16 05:00 [medline]
PHST- 2003/09/02 05:00 [entrez]
PST - ppublish
SO  - Sichuan Da Xue Xue Bao Yi Xue Ban. 2003 Apr;34(2):333-6.