PMID- 1364339 OWN - NLM STAT- MEDLINE DCOM- 19941108 LR - 20131121 IS - 0077-4715 (Print) IS - 0077-4715 (Linking) IP - 108 DP - 1990 TI - [Studies on the identification of psychotropic substances (VII). Preparation and various analytical data of standard references of some hallucinogens, 3,4-methylenedioxyamphetamine (MDA), 3,4- methylenedioxymethamphetamine (MDMA) and 5-methoxy-3,4- methylenedioxyamphetamine (MMDA)]. PG - 118-25 AB - The Reference Standards of 3, 4-methylenedioxyamphetamine (MDA), 3, 4-methylenedioxymethamphetamine (MDMA) and 5-methoxy-3,4-methylenedioxyamphetamine (MMDA) were prepared. Their purities determined by HPLC were 99.8% for DMA hydrochloride, 99.8% for MDMA hydrochloride and 99.5% for MMDA hydrochloride. For the identification and determination, various analytical data of the three drugs were measured and studied by TLC, UV, IR, HPLC, GC/MS and NMR. FAU - Shimamine, M AU - Shimamine M FAU - Takahashi, K AU - Takahashi K FAU - Nakahara, Y AU - Nakahara Y LA - jpn PT - English Abstract PT - Journal Article PL - Japan TA - Eisei Shikenjo Hokoku JT - Eisei Shikenjo hokoku. Bulletin of National Institute of Hygienic Sciences JID - 0421152 RN - 13674-05-0 (MMDA) RN - 4764-17-4 (3,4-Methylenedioxyamphetamine) RN - KE1SEN21RM (N-Methyl-3,4-methylenedioxyamphetamine) SB - IM MH - 3,4-Methylenedioxyamphetamine/*analogs & derivatives/isolation & purification/*standards MH - Chromatography, High Pressure Liquid MH - Chromatography, Thin Layer MH - Gas Chromatography-Mass Spectrometry MH - N-Methyl-3,4-methylenedioxyamphetamine/isolation & purification/*standards MH - Spectrophotometry EDAT- 1990/01/01 00:00 MHDA- 1990/01/01 00:01 CRDT- 1990/01/01 00:00 PHST- 1990/01/01 00:00 [pubmed] PHST- 1990/01/01 00:01 [medline] PHST- 1990/01/01 00:00 [entrez] PST - ppublish SO - Eisei Shikenjo Hokoku. 1990;(108):118-25.