PMID- 14669694 OWN - NLM STAT- MEDLINE DCOM- 20040123 LR - 20201208 IS - 0324-8267 (Print) IS - 0324-8267 (Linking) VI - 52 IP - 3 DP - 2002 Jul-Sep TI - [Analytical problems in examination of small amounts of blood samples taken from law offenders]. PG - 229-39 AB - In the paper there have presented results of the analysis of small blood samples taken routinely from 3 cases after car accidents and 1 rapist. Fluorescence polarisation immunoassay (FPIA, Abott) was used for screening examinations of narcotics from the group of both opium and cocaine alkaloids, barbituric acid and benzodiazepine and also drugs from the group of tricyclic antidepressants. Confirmation of the obtained results and full identification of the substances analysed were carried out by liquid chromatography with mass spectrometry (LC-MS). In the causes of car accidents components of "compote" were found (poppy straw extract) morphine and codeine (1 case), cocaine (1 case) and also tramadol and diazepam (1 case) were also found. In the rapist methylenedioxymethamphetamine (MDMA) was determined. FAU - Celinski, Rafal AU - Celinski R AD - Katedry Medycyny Sadowej Slaskiej AM w Katowicach. FAU - Kulikowska, Joanna AU - Kulikowska J FAU - Albert, Malgorzata AU - Albert M FAU - Sybirska, Halina AU - Sybirska H LA - pol PT - Case Reports PT - Journal Article TT - Problemy analityczne w badaniach malych probek krwi pobranych od osob, ktore zlamaly prawo. PL - Poland TA - Arch Med Sadowej Kryminol JT - Archiwum medycyny sadowej i kryminologii JID - 1260766 RN - 0 (Analgesics, Opioid) RN - 0 (Anti-Anxiety Agents) RN - 0 (Designer Drugs) RN - 0 (Narcotics) RN - 39J1LGJ30J (Tramadol) RN - 76I7G6D29C (Morphine) RN - I5Y540LHVR (Cocaine) RN - KE1SEN21RM (N-Methyl-3,4-methylenedioxyamphetamine) RN - Q3JTX2Q7TU (Diazepam) RN - UX6OWY2V7J (Codeine) SB - IM MH - Accidents, Traffic MH - Analgesics, Opioid/*blood MH - Anti-Anxiety Agents/*blood MH - Chromatography, Liquid/methods MH - Cocaine/blood MH - Codeine/blood MH - Designer Drugs/*metabolism MH - Diazepam/blood MH - Fluorescence Polarization Immunoassay/methods MH - Gas Chromatography-Mass Spectrometry/methods MH - Humans MH - Male MH - Morphine/blood MH - N-Methyl-3,4-methylenedioxyamphetamine/blood MH - Narcotics/*blood MH - Rape MH - Sensitivity and Specificity MH - Substance Abuse Detection/*methods MH - Tramadol/blood EDAT- 2003/12/13 05:00 MHDA- 2004/01/24 05:00 CRDT- 2003/12/13 05:00 PHST- 2003/12/13 05:00 [pubmed] PHST- 2004/01/24 05:00 [medline] PHST- 2003/12/13 05:00 [entrez] PST - ppublish SO - Arch Med Sadowej Kryminol. 2002 Jul-Sep;52(3):229-39.