PMID- 15154980
OWN - NLM
STAT- MEDLINE
DCOM- 20040712
LR  - 20190513
IS  - 0021-9665 (Print)
IS  - 0021-9665 (Linking)
VI  - 42
IP  - 4
DP  - 2004 Apr
TI  - Microwave-assisted extraction and quantitative analysis of high-density 
      polyethylene pellets fortified with flavors.
PG  - 191-5
AB  - Microwave-assisted extraction (MAE) has been shown to be an easy, rapid, 
      accurate, quantitative, and precise component of an overall method for the 
      quantitative analysis of flavor components formulated into high-density 
      polyethylene (HDPE) pellets. Under optimized extraction conditions, MAE can be 
      perform extraction of flavors from pellets within 1/2 h with flavor recoveries 
      ranging from approximately 90% to 100%. The variability in the data expressed as 
      percent relative standard deviation from gas chromatographic-mass selective 
      detector analysis of targeted flavor components is always less than 5%, 
      indicating a precise method. In addition, the major components identified in the 
      flavor formulation prior to formulation into the HDPE pellets are the major 
      components detected in the extraction, indicating an accurate determination. 
      Thus, MAE can be readily recommended as an essential component of a high-volume 
      approach to the quantitative determination of flavors formulated into HDPE 
      pellets.
FAU - Coleman, W M 3rd
AU  - Coleman WM 3rd
AD  - R.J. Reynolds Tobacco Company, P.O. Box 1487, Winston Salem, NC 27102-1487, USA. 
      colemaw@rjrt.com
FAU - Crumpler, L A
AU  - Crumpler LA
LA  - eng
PT  - Journal Article
PL  - United States
TA  - J Chromatogr Sci
JT  - Journal of chromatographic science
JID - 0173225
RN  - 0 (Flavoring Agents)
RN  - 0 (Polyethylenes)
SB  - IM
MH  - Flavoring Agents/*analysis
MH  - Gas Chromatography-Mass Spectrometry
MH  - Microwaves
MH  - Polyethylenes/*analysis
MH  - Reference Standards
EDAT- 2004/05/25 05:00
MHDA- 2004/07/13 05:00
CRDT- 2004/05/25 05:00
PHST- 2004/05/25 05:00 [pubmed]
PHST- 2004/07/13 05:00 [medline]
PHST- 2004/05/25 05:00 [entrez]
AID - 10.1093/chromsci/42.4.191 [doi]
PST - ppublish
SO  - J Chromatogr Sci. 2004 Apr;42(4):191-5. doi: 10.1093/chromsci/42.4.191.