PMID- 15348153 OWN - NLM STAT- PubMed-not-MEDLINE DCOM- 20050228 LR - 20191026 IS - 0957-4530 (Print) IS - 0957-4530 (Linking) VI - 10 IP - 4 DP - 1999 Apr TI - Incorporation of a controlled-release glass into a calcium phosphate cement. PG - 215-8 AB - A so-called controlled-release glass was synthesized occurring in the system CaO-Na2O-P2O5. A certain sieve fraction of this glass was incorporated in a calcium phosphate cement, of which the powder contained alpha-tricalcium phosphate (alpha-TCP), dicalcium phosphate (DCP) and precipitated hydroxyapatite (HA). The glass appeared to retard the cement setting slightly and it reduced considerably the compressive strength after aging in aqueous solutions which were continuously refreshed. Scanning electron microscope (SEM) pictures and X-ray diffraction (XRD) patterns of the samples after 5 weeks of aging showed that the glass was not dissolved but that large brushite crystals were formed. Thereby, aging in CaCl2 solutions resulted in more brushite formation than aging in NaCl solutions. The brushite crystals did not reinforce the cement. Neither was the aged glass-containing cement weaker than it was before the brushite formation right after complete setting. In conclusion, the incorporation of controlled-release glasses into a calcium phosphate cement and subsequent aging in aqueous solutions did not result in the formation of macropores in the cement structure, but that of brushite crystals. This incorporation reduced the compressive strength of the cement considerably. CI - Copyright 1999 Kluwer Academic Publishers FAU - Khairoun, I AU - Khairoun I AD - Department of Materials Science and Metallurgy, Universitat Politecnica de Catalunya, Avda. Diagonal 647, E-08028, Barcelona, Spain. FAU - Boltong, M G AU - Boltong MG FAU - Gil, F J AU - Gil FJ FAU - Driessens, F C AU - Driessens FC FAU - Planell, J A AU - Planell JA FAU - Seijas, M M AU - Seijas MM FAU - Martinez, S AU - Martinez S LA - eng PT - Journal Article PL - United States TA - J Mater Sci Mater Med JT - Journal of materials science. Materials in medicine JID - 9013087 EDAT- 2004/09/07 05:00 MHDA- 2004/09/07 05:01 CRDT- 2004/09/07 05:00 PHST- 2004/09/07 05:00 [pubmed] PHST- 2004/09/07 05:01 [medline] PHST- 2004/09/07 05:00 [entrez] AID - 234728 [pii] AID - 10.1023/a:1008954011349 [doi] PST - ppublish SO - J Mater Sci Mater Med. 1999 Apr;10(4):215-8. doi: 10.1023/a:1008954011349.