PMID- 15813375
OWN - NLM
STAT- MEDLINE
DCOM- 20050628
LR  - 20191021
IS  - 0939-5075 (Print)
IS  - 0341-0382 (Linking)
VI  - 59
IP  - 7-8
DP  - 2004 Jul-Aug
TI  - Analysis of Rhioxma Curcumae Aeruginosae volatiles by solid-phase microextraction 
      with gas chromatography-mass spectrometry.
PG  - 533-7
AB  - In this paper, a headspace solid-phase microextraction (HS-SPME) method was 
      applied to analyse the volatile compounds in a traditional Chinese medicine 
      (TCM), Rhioxma Curcumae Aeruginosae. SPME parameters such as fibers, extraction 
      temperature, extraction time and desorption time were investigated. Thirty-five 
      volatile compounds were separated and identified. Relative standard deviations 
      (RSDs) were less than 8.4%, showing that the method has a good reproducibility. 
      The volatile constituents were also analyzed by steam distillation (SD) and 
      thirty-seven compounds were identified. The similar results obtained by the two 
      methods showed that SPME is a good alternative for the analysis of volatile 
      constituents in Rhioxma Curcumae Aeruginosae samples and it is a relatively 
      simple, rapid and solvent-free method.
FAU - Sha, Yun F
AU  - Sha YF
AD  - Department of Pharmacy, Fudan University, Shanghai 200032, People's Republic of 
      China.
FAU - Shen, Shun
AU  - Shen S
FAU - Duan, Geng L
AU  - Duan GL
LA  - eng
PT  - Journal Article
PL  - Germany
TA  - Z Naturforsch C J Biosci
JT  - Zeitschrift fur Naturforschung. C, Journal of biosciences
JID - 8912155
RN  - 0 (Drugs, Chinese Herbal)
RN  - 0 (Oils, Volatile)
RN  - 0 (Plant Extracts)
RN  - 76-22-2 (Camphor)
SB  - IM
MH  - Camphor/chemistry/isolation & purification
MH  - China
MH  - Drugs, Chinese Herbal/*chemistry/isolation & purification
MH  - Gas Chromatography-Mass Spectrometry
MH  - Medicine, Chinese Traditional
MH  - Oils, Volatile/*chemistry/*isolation & purification
MH  - Plant Extracts/*chemistry/isolation & purification
EDAT- 2005/04/09 09:00
MHDA- 2005/06/29 09:00
CRDT- 2005/04/09 09:00
PHST- 2005/04/09 09:00 [pubmed]
PHST- 2005/06/29 09:00 [medline]
PHST- 2005/04/09 09:00 [entrez]
AID - 10.1515/znc-2004-7-815 [doi]
PST - ppublish
SO  - Z Naturforsch C J Biosci. 2004 Jul-Aug;59(7-8):533-7. doi: 
      10.1515/znc-2004-7-815.