PMID- 15974079
OWN - NLM
STAT- MEDLINE
DCOM- 20050926
LR  - 20190720
IS  - 0021-9673 (Print)
IS  - 0021-9673 (Linking)
VI  - 1076
IP  - 1-2
DP  - 2005 May 27
TI  - Analysis of potential and free furfural compounds in milk-based formulae by 
      high-performance liquid chromatography. Evolution during storage.
PG  - 133-40
AB  - A simple and reproducible HPLC-diode array detection method for the qualitative 
      and quantitative analysis of potential and free furfural compounds 
      (5-hydroxymethyl-2-furaldehyde, HMF; 2-furaldehyde, F; 2-furyl methyl ketone, 
      FMC; and 5-methyl-2-furaldehyde, MF) in milk-based formulae was developed and 
      validated. The method showed good linearity with determination coefficients over 
      0.999. The limits of detection and quantification were acceptable for all 
      furfurals. The relative standard deviations (RSDs) for repeatability and 
      reproducibility were <4.28. Recoveries in all furfurals were between 94.5 and 
      98.7%. In addition, we report the evolution over shelf life of furfural compound 
      levels in an experimental powder formula for pregnant women stored at 25 and 37 
      degrees C from production until 15 months.
FAU - Chavez-Servin, Jorge L
AU  - Chavez-Servin JL
AD  - Dpt. Nutricio i Bromatologia, Centre de Referencia en Tecnologia dels Aliments 
      (CeRTA), Facultat de Farmacia, Universitat de Barcelona, Avda. Joan XXIII s/n, 
      E-08028 Barcelona, Spain.
FAU - Castellote, Ana I
AU  - Castellote AI
FAU - Lopez-Sabater, M Carmen
AU  - Lopez-Sabater MC
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
PL  - Netherlands
TA  - J Chromatogr A
JT  - Journal of chromatography. A
JID - 9318488
RN  - DJ1HGI319P (Furaldehyde)
SB  - IM
MH  - Animals
MH  - Chromatography, High Pressure Liquid/*methods
MH  - Furaldehyde/*analysis
MH  - Humans
MH  - Infant
MH  - Infant Food/*analysis
MH  - Milk/*chemistry
MH  - Reproducibility of Results
MH  - Sensitivity and Specificity
EDAT- 2005/06/25 09:00
MHDA- 2005/09/27 09:00
CRDT- 2005/06/25 09:00
PHST- 2005/06/25 09:00 [pubmed]
PHST- 2005/09/27 09:00 [medline]
PHST- 2005/06/25 09:00 [entrez]
AID - S0021-9673(05)00805-8 [pii]
AID - 10.1016/j.chroma.2005.04.046 [doi]
PST - ppublish
SO  - J Chromatogr A. 2005 May 27;1076(1-2):133-40. doi: 10.1016/j.chroma.2005.04.046.