PMID- 16100747
OWN - NLM
STAT- MEDLINE
DCOM- 20060420
LR  - 20131121
IS  - 1522-7235 (Print)
IS  - 1522-7235 (Linking)
VI  - 21
IP  - 1
DP  - 2006 Jan-Feb
TI  - Flow-injection determination of streptomycin residues in milk using the 
      luminol-periodate-Mn2+ chemiluminescence system.
PG  - 36-42
AB  - A novel flow-injection method with chemiluminescence detection was developed for 
      the determination of streptomycin residues in milk, based on the enhancement by 
      streptomycin of the luminol-potassium periodate-Mn(2+) chemiluminescence system. 
      The assay allowed analysis of streptomycin residues in whole milk samples ( 
      approximately 3.5% fat) after sample work-up procedures. The limit of detection 
      was 5.16 x 10(-9) mol/L for milk, and was far below the regulations of maximum 
      residue limits (MRLs). The relative standard deviation (RSD) for 8.66 x 10(-8) 
      mol/L streptomycin was 1.94% (n = 15) in milk. The results obtained for the assay 
      of streptomycin residues in milk was comparable with those obtained by the 
      official methods (ELISA) and demonstrated good accuracy and precision. The 
      possible mechanism is briefly discussed.
FAU - Wan, Guo-Hui
AU  - Wan GH
AD  - Department of Chemistry, University of Science and Technology of China, Hefei, 
      Anhui 230026, People's Republic of China.
FAU - Cui, Hua
AU  - Cui H
FAU - Zheng, Hai-Song
AU  - Zheng HS
FAU - Pang, Yong-Qiang
AU  - Pang YQ
FAU - Liu, Li-Juan
AU  - Liu LJ
FAU - Yu, Xiao-Feng
AU  - Yu XF
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
PL  - England
TA  - Luminescence
JT  - Luminescence : the journal of biological and chemical luminescence
JID - 100889025
RN  - 0 (Anti-Bacterial Agents)
RN  - 10450-60-9 (Periodic Acid)
RN  - 42Z2K6ZL8P (Manganese)
RN  - 5EXP385Q4F (Luminol)
RN  - Y45QSO73OB (Streptomycin)
SB  - IM
MH  - Animals
MH  - Anti-Bacterial Agents/*analysis
MH  - Drug Residues/*analysis
MH  - Flow Injection Analysis/*methods
MH  - Kinetics
MH  - Luminol/*chemistry
MH  - Manganese/*chemistry
MH  - Milk/*chemistry
MH  - Periodic Acid/*chemistry
MH  - Streptomycin/*analysis
EDAT- 2005/08/16 09:00
MHDA- 2006/04/21 09:00
CRDT- 2005/08/16 09:00
PHST- 2005/08/16 09:00 [pubmed]
PHST- 2006/04/21 09:00 [medline]
PHST- 2005/08/16 09:00 [entrez]
AID - 10.1002/bio.880 [doi]
PST - ppublish
SO  - Luminescence. 2006 Jan-Feb;21(1):36-42. doi: 10.1002/bio.880.