PMID- 16196130
OWN - NLM
STAT- MEDLINE
DCOM- 20051031
LR  - 20191210
IS  - 0021-9673 (Print)
IS  - 0021-9673 (Linking)
VI  - 1090
IP  - 1-2
DP  - 2005 Oct 7
TI  - Determination of pesticides in compost by pressurized liquid extraction and gas 
      chromatography-mass spectrometry.
PG  - 10-5
AB  - A gas chromatographic-mass spectrometric method was developed for the 
      determination of pesticides in compost. The investigated pesticides included two 
      fungicides, two herbicides and 10 insecticides. The pesticides were extracted 
      from the compost by pressurized liquid extraction. The extract was cleaned up by 
      a partition between hexane and acetonitrile followed by a dispersive solid-phase 
      extraction using a porous carbon made from Moso bamboo (Phyllostachys pubescens). 
      The overall recoveries were 81-104% and the relative standard deviations (RSDs) 
      ranged from 2.4 to 12%. The minimum detectable concentrations were 0.02-0.04 
      microg g(-1). This method was successfully applied to a compost sample from food 
      waste as well as commercial compost.
FAU - Kawata, Kuniaki
AU  - Kawata K
AD  - Faculty of Applied Life Sciences, Niigata University of Pharmacy and Applied Life 
      Sciences, 265-1 Higashijima, Niigata 956-8603, Japan. kawata@niigatayakudai.jp
FAU - Asada, Takashi
AU  - Asada T
FAU - Oikawa, Kikuo
AU  - Oikawa K
LA  - eng
PT  - Evaluation Study
PT  - Journal Article
PT  - Validation Study
PL  - Netherlands
TA  - J Chromatogr A
JT  - Journal of chromatography. A
JID - 9318488
RN  - 0 (Fungicides, Industrial)
RN  - 0 (Herbicides)
RN  - 0 (Insecticides)
RN  - 0 (Pesticides)
RN  - 0 (Soil)
RN  - 0 (Soil Pollutants)
SB  - IM
MH  - Chemical Fractionation/methods
MH  - Fungicides, Industrial/analysis
MH  - Gas Chromatography-Mass Spectrometry/methods
MH  - Herbicides/analysis
MH  - Insecticides/analysis
MH  - Pesticides/*analysis
MH  - Pressure
MH  - Soil/*analysis
MH  - Soil Pollutants/analysis
EDAT- 2005/10/01 09:00
MHDA- 2005/11/01 09:00
CRDT- 2005/10/01 09:00
PHST- 2005/10/01 09:00 [pubmed]
PHST- 2005/11/01 09:00 [medline]
PHST- 2005/10/01 09:00 [entrez]
AID - S0021-9673(05)01425-1 [pii]
AID - 10.1016/j.chroma.2005.07.011 [doi]
PST - ppublish
SO  - J Chromatogr A. 2005 Oct 7;1090(1-2):10-5. doi: 10.1016/j.chroma.2005.07.011.