PMID- 16298182
OWN - NLM
STAT- MEDLINE
DCOM- 20060109
LR  - 20131121
IS  - 0021-9673 (Print)
IS  - 0021-9673 (Linking)
VI  - 1097
IP  - 1-2
DP  - 2005 Dec 2
TI  - Simultaneous determination of tetrabromobisphenol A, tetrachlorobisphenol A, 
      bisphenol A and other halogenated analogues in sediment and sludge by high 
      performance liquid chromatography-electrospray tandem mass spectrometry.
PG  - 25-32
AB  - A high performance liquid chromatography-electrospray (negative) 
      ionization-tandem mass spectrometry (HPLC-ESI(-)-MS-MS) based method has been 
      developed for simultaneous determination of bisphenol A (BPA), 
      tetrachlorobisphenol A (TCBPA), and tetrabromobisphenol A (TBBPA), as well as 
      lower brominated BPA analogues in sediment and sludge samples. Samples were 
      extracted with MTBE, target compounds were partitioned by aqueous solution of 
      sodium hydroxide. The solution was subsequently acidified, and the enrichment and 
      desalting were performed via solid phase extraction (SPE). After cleanup the 
      target compounds were determined by HPLC-ESI(-)-MS-MS. The method limits of 
      quantification (MLOQs) from sediment and sludge for BPA, monobromo-bisphenol A 
      (mono-BBPA), dibromo-bisphenol A (di-BBPA), tribromo-bisphenol A (tri-BBPA), 
      TBBPA and TCBPA were 0.15, 0.02, 0.02, 0.04, 0.05, and 0.03 ng/g (dry weight), 
      respectively. Mean recovery of the analytes from spiked samples ranged from 70 to 
      105%, and the relative standard deviation ranged from 4.9 to 13.1%. The method 
      was successfully applied to sediment and sludge samples analysis.
FAU - Chu, Shaogang
AU  - Chu S
AD  - Great Lakes Institute for Environmental Research, University of Windsor, 401 
      Sunset Avenue, Windsor, Ont., Canada N9B 3P4.
FAU - Haffner, G Douglas
AU  - Haffner GD
FAU - Letcher, Robert J
AU  - Letcher RJ
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
DEP - 20050819
PL  - Netherlands
TA  - J Chromatogr A
JT  - Journal of chromatography. A
JID - 9318488
RN  - 0 (Benzhydryl Compounds)
RN  - 0 (Chlorophenols)
RN  - 0 (Hydrocarbons, Halogenated)
RN  - 0 (Phenols)
RN  - 0 (Polybrominated Biphenyls)
RN  - 0 (Sewage)
RN  - 0 (Water Pollutants, Chemical)
RN  - FO0P9ET4BN (tetrachlorodian)
RN  - FQI02RFC3A (tetrabromobisphenol A)
RN  - MLT3645I99 (bisphenol A)
SB  - IM
MH  - Benzhydryl Compounds
MH  - Chlorophenols/analysis
MH  - Chromatography, High Pressure Liquid/*methods
MH  - Geologic Sediments/*chemistry
MH  - Hydrocarbons, Halogenated/analysis
MH  - Phenols/analysis
MH  - Polybrominated Biphenyls/analysis
MH  - Reproducibility of Results
MH  - Sewage/*chemistry
MH  - Spectrometry, Mass, Electrospray Ionization/*methods
MH  - Water Pollutants, Chemical/*analysis
EDAT- 2005/11/22 09:00
MHDA- 2006/01/10 09:00
CRDT- 2005/11/22 09:00
PHST- 2005/06/07 00:00 [received]
PHST- 2005/07/27 00:00 [revised]
PHST- 2005/08/03 00:00 [accepted]
PHST- 2005/11/22 09:00 [pubmed]
PHST- 2006/01/10 09:00 [medline]
PHST- 2005/11/22 09:00 [entrez]
AID - S0021-9673(05)01630-4 [pii]
AID - 10.1016/j.chroma.2005.08.007 [doi]
PST - ppublish
SO  - J Chromatogr A. 2005 Dec 2;1097(1-2):25-32. doi: 10.1016/j.chroma.2005.08.007. 
      Epub 2005 Aug 19.