PMID- 16358704
OWN - NLM
STAT- MEDLINE
DCOM- 20100420
LR  - 20191210
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 20
IP  - 5
DP  - 2002 Sep
TI  - [Determination of oxolinic acid residues in baked and fresh eels by high 
      performance liquid chromatography without derivatization].
PG  - 462-3
AB  - A method for rapid determination of oxolinic acid residues in baked eels and 
      fresh eels by high performance liquid chromatography without derivatization was 
      studied. The samples were triturated, and extracted with methylene dichloride. 
      The extracted solutions were evaporated to dryness, and then was dissolved by 
      using the mobil phase. The solutions were cleaned-up by partition with n-hexane 
      before analysis. The components were analysed on a Nova-Pak C18 column (150 mm x 
      3.9 mm i.d., 5 microm), with methanol-diluted phosphoric acid (pH 2.5) (40:60, 
      V/V) as the mobile phose at a flow rate of 0.8 mL/min and detected by a 
      fluorescence detector at the excitation wavelength (lambdaex) 254 nm and the 
      emission wavelength (lambdaem) 375 nm. The detection limit was 0.01 mg/kg (S/N = 
      3). The recoveries were over 80 %, and the relative standard deviations (RSDs) 
      were less than 3.8%.
FAU - Chen, Xiao-Mei
AU  - Chen XM
AD  - Zhejiang Enter-Exit Inspection and Quarantine Bureau, Hangzhou 310012, China.
FAU - Shi, Xu-Xia
AU  - Shi XX
LA  - chi
PT  - Evaluation Study
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Anti-Infective Agents)
RN  - 0 (Veterinary Drugs)
RN  - L0A22B22FT (Oxolinic Acid)
SB  - IM
MH  - Animals
MH  - Anti-Infective Agents/analysis
MH  - Chromatography, High Pressure Liquid/*methods
MH  - Drug Residues/*analysis
MH  - *Eels
MH  - Food Contamination/analysis
MH  - Food Handling
MH  - Oxolinic Acid/*analysis
MH  - Seafood/*analysis
MH  - Veterinary Drugs/*analysis
EDAT- 2005/12/20 09:00
MHDA- 2010/04/21 06:00
CRDT- 2005/12/20 09:00
PHST- 2005/12/20 09:00 [pubmed]
PHST- 2010/04/21 06:00 [medline]
PHST- 2005/12/20 09:00 [entrez]
PST - ppublish
SO  - Se Pu. 2002 Sep;20(5):462-3.