PMID- 16815764
OWN - NLM
STAT- MEDLINE
DCOM- 20061229
LR  - 20061031
IS  - 1570-0232 (Print)
IS  - 1570-0232 (Linking)
VI  - 843
IP  - 2
DP  - 2006 Nov 7
TI  - Development of an analytical method for organotin compounds in fortified flour 
      samples using microwave-assisted extraction and normal-phase HPLC with UV 
      detection.
PG  - 268-74
AB  - The normal high-performance liquid chromatography with UV detection was applied 
      for the determination of tributyltin chloride (TBT), triphenyltin chloride 
      (TPhT), tetraphenyltin (TrPhT), triethyltin chloride (TET) and tetraethyltin 
      (TrET) from flour samples. The separation was performed in the isocratic mode on 
      cyanopropyl column with a mobile phase of hexane-acetonitrile-THF (97/1/2). Under 
      the experimental conditions used, quantitative limit of TBT, TPhT, TrPhT, TET and 
      TrET are 0.95, 0.46, 0.97, 0.75 and 0.96 microg/ml, respectively. 
      Microwave-assisted extraction of organotin (OT) compounds at 100 degrees C with 
      an extraction time of 3 min was described. The extraction of organotin can be 
      finished in acetic acid-hexane (20/80) medium. The quantitative extraction of 
      five organotin compounds was achieved with recoveries ranging from 88 to 101% 
      R.S.D. 3-8%.
FAU - Wang, Xiupin
AU  - Wang X
AD  - College of Chemistry, Jilin University, Changchun 130012, PR China.
FAU - Ding, Lan
AU  - Ding L
FAU - Zhang, Huarong
AU  - Zhang H
FAU - Cheng, Jianhua
AU  - Cheng J
FAU - Yu, Aimin
AU  - Yu A
FAU - Zhang, Hanqi
AU  - Zhang H
FAU - Liu, Li
AU  - Liu L
FAU - Liu, Zhihong
AU  - Liu Z
FAU - Li, Ying
AU  - Li Y
LA  - eng
PT  - Journal Article
DEP - 20060703
PL  - Netherlands
TA  - J Chromatogr B Analyt Technol Biomed Life Sci
JT  - Journal of chromatography. B, Analytical technologies in the biomedical and life 
      sciences
JID - 101139554
RN  - 0 (Organotin Compounds)
SB  - IM
MH  - Analytic Sample Preparation Methods/*methods
MH  - Chromatography, High Pressure Liquid/*methods
MH  - Flour/*analysis
MH  - Food, Fortified/*analysis
MH  - Microwaves
MH  - Organotin Compounds/*analysis
MH  - Ultraviolet Rays
EDAT- 2006/07/04 09:00
MHDA- 2006/12/30 09:00
CRDT- 2006/07/04 09:00
PHST- 2005/12/16 00:00 [received]
PHST- 2006/06/07 00:00 [revised]
PHST- 2006/06/12 00:00 [accepted]
PHST- 2006/07/04 09:00 [pubmed]
PHST- 2006/12/30 09:00 [medline]
PHST- 2006/07/04 09:00 [entrez]
AID - S1570-0232(06)00473-9 [pii]
AID - 10.1016/j.jchromb.2006.06.013 [doi]
PST - ppublish
SO  - J Chromatogr B Analyt Technol Biomed Life Sci. 2006 Nov 7;843(2):268-74. doi: 
      10.1016/j.jchromb.2006.06.013. Epub 2006 Jul 3.