PMID- 17580693
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20100615
LR  - 20161018
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 25
IP  - 2
DP  - 2007 Mar
TI  - [Determination of major carbonyls in mainstream smoke by rapid column high 
      performance liquid chromatography].
PG  - 230-3
AB  - Abstract: The determination of major carbonyl compounds in mainstream cigarette 
      smoke by rapid column high performance liquid chromatography was investigated. 
      The cigarette smoke was collected using a Cambridge filter treated with acidic 
      solution of 2, 4-dinitrophenyl-hydrazine. Formaldehyde, acetaldehyde, acetone, 
      acrolein, propionaldehyde, crotonaldehyde, 2-butanone and butyraldehyde were 
      extracted from the Cambridge filter with 50 mL of 2% pyridine acetonitrile 
      solution. The carbonyl compounds in samples were separated on a ZORBAX Stable 
      Bound rapid column (50 mm x 4. 6 mm, 1. 8 microm) in approximately seven minutes 
      and then determined by high performance liquid chromatography with a diode array 
      detector. The average recoveries were in the range of 89. 1% to 99. 2% and the 
      relative standard deviations (RSDs) were generally below 6. 0%. The eight 
      carbonyl compounds in the mainstream smoke of five brands of cigarettes were 
      determined using this method. This method is faster, simpler and consumes less 
      solvent. It is suitable for rapid analysis of carbonyl compounds in mainstream 
      cigarette smoke.
FAU - Huang, Yun
AU  - Huang Y
AD  - School of Chemical Science and Technology of Yunnan University, Kunming 650091, 
      China.
FAU - Wang, Yigeng
AU  - Wang Y
FAU - Miao, Mingming
AU  - Miao M
FAU - Zhao, Qihua
AU  - Zhao Q
FAU - Yang, Guangyu
AU  - Yang G
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
EDAT- 2007/06/22 09:00
MHDA- 2007/06/22 09:01
CRDT- 2007/06/22 09:00
PHST- 2007/06/22 09:00 [pubmed]
PHST- 2007/06/22 09:01 [medline]
PHST- 2007/06/22 09:00 [entrez]
PST - ppublish
SO  - Se Pu. 2007 Mar;25(2):230-3.