PMID- 17680171
OWN - NLM
STAT- MEDLINE
DCOM- 20071127
LR  - 20091111
IS  - 0007-4861 (Print)
IS  - 0007-4861 (Linking)
VI  - 79
IP  - 2
DP  - 2007 Aug
TI  - Determination of toxaphene residues in fish foodstuff by GC-MS.
PG  - 226-30
AB  - A method for the determination of toxaphene residues in fish and fish-based baby 
      foods has been developed. The cleanup of the fatty matrices was performed using 
      an acid treatment on an Extrelut-NT3 and ENVI-Florisil SPE cartridges system, 
      using light petroleum as eluent. Instrumental analysis was carried out by 
      gaschromatography with mass spectrometry detector (GC/MS) in SIM mode. Recoveries 
      from spiked samples were tested at 0.005 and 0.01 mg/kg per single congener and 
      were in the range 82-104% while relative standard deviations (RSDs) were in the 
      range 3.7-10.9%. Nineteen samples of both frozen fish food and fish-based baby 
      foods representative of the Italian market were collected from local dealers and 
      analysed.
FAU - Barbini, D Attard
AU  - Barbini DA
AD  - Dipartimento Ambiente e Connessa Prevenzione Primaria, ISS, Istituto Superiore di 
      Sanita, viale Regina Elena, 299, 00161 Rome, Italy. danilo.attardbarbini@iss.it
FAU - Stefanelli, P
AU  - Stefanelli P
FAU - Girolimetti, S
AU  - Girolimetti S
FAU - Di Muccio, A
AU  - Di Muccio A
FAU - Dommarco, R
AU  - Dommarco R
LA  - eng
PT  - Journal Article
DEP - 20070807
PL  - United States
TA  - Bull Environ Contam Toxicol
JT  - Bulletin of environmental contamination and toxicology
JID - 0046021
RN  - 0 (Insecticides)
RN  - 0 (Pesticide Residues)
RN  - 0 (Water Pollutants, Chemical)
RN  - 8001-35-2 (Toxaphene)
SB  - IM
MH  - Animals
MH  - Fish Products/*analysis
MH  - Food Contamination/*analysis
MH  - Gas Chromatography-Mass Spectrometry
MH  - Infant Food/analysis
MH  - Insecticides/*analysis
MH  - Italy
MH  - Pesticide Residues/*analysis
MH  - Toxaphene/*analysis
MH  - Water Pollutants, Chemical/*analysis
EDAT- 2007/08/08 09:00
MHDA- 2007/12/06 09:00
CRDT- 2007/08/08 09:00
PHST- 2007/02/12 00:00 [received]
PHST- 2007/06/01 00:00 [accepted]
PHST- 2007/08/08 09:00 [pubmed]
PHST- 2007/12/06 09:00 [medline]
PHST- 2007/08/08 09:00 [entrez]
AID - 10.1007/s00128-007-9179-6 [doi]
PST - ppublish
SO  - Bull Environ Contam Toxicol. 2007 Aug;79(2):226-30. doi: 
      10.1007/s00128-007-9179-6. Epub 2007 Aug 7.