PMID- 17763032 OWN - NLM STAT- MEDLINE DCOM- 20071206 LR - 20191110 IS - 0360-1234 (Print) IS - 0360-1234 (Linking) VI - 42 IP - 7 DP - 2007 Sep-Oct TI - Dissipation of fenoxycarb and pyriproxyfen in fresh and canned peach. PG - 767-73 AB - The objective of this work was to determine the dissipation of fenoxycarb and pyriproxyfen in fresh and canned peaches in order to know the levels of residues that can reach consumers in real circumstances. Two field dissipation studies were carried out, one of them at the pre-harvest interval (PHI) with good agricultural practice (GAP) and the other one in a situation of critical agricultural practice (CAP). Two canning dissipation studies were carried out for samples from both agricultural situations in an industrial pilot plant and the dissipation was determined in each relevant step. An analytical methodology was used including acetone-dichloromethane extraction, purification and analysis by liquid chromatography and diode array detection (LC-DAD) with a limit of quantification (LOQ) of 0.05 mg/kg. It was validated under SANCO/10232/2006 Guidelines. These pesticides complied with the official maximum residue limits (MRLs) in peaches at the PHI with good agricultural practices. In hypothetical situation of a second application at the PHI, fenoxycarb and pyriproxyfen residues were above the MRLs in peaches. The canning study reduced the residues to no detectable levels in the cans for consumers. FAU - Paya, Paula AU - Paya P AD - Departamento de Quimica Agricola, Geologia y Edafologia, Facultad de Quimica, Universidad de Murcia, Murcia, Spain. FAU - Oliva, Jose AU - Oliva J FAU - Camara, Miguel A AU - Camara MA FAU - Barba, Alberto AU - Barba A LA - eng PT - Journal Article PT - Research Support, Non-U.S. Gov't PL - England TA - J Environ Sci Health B JT - Journal of environmental science and health. Part. B, Pesticides, food contaminants, and agricultural wastes JID - 7607167 RN - 0 (Insecticides) RN - 0 (Pesticide Residues) RN - 0 (Phenylcarbamates) RN - 0 (Pyridines) RN - 3Q9VOR705O (pyriproxyfen) RN - JEN0LSV1G9 (fenoxycarb) SB - IM MH - Agriculture/methods/standards MH - Chromatography, Liquid MH - *Consumer Product Safety MH - Food Contamination/analysis MH - Food Preservation/*methods MH - Humans MH - Insecticides/analysis MH - Pesticide Residues/*analysis MH - Phenylcarbamates/*analysis MH - Prunus/*chemistry MH - Pyridines/*analysis EDAT- 2007/09/01 09:00 MHDA- 2007/12/07 09:00 CRDT- 2007/09/01 09:00 PHST- 2007/09/01 09:00 [pubmed] PHST- 2007/12/07 09:00 [medline] PHST- 2007/09/01 09:00 [entrez] AID - 781711449 [pii] AID - 10.1080/03601230701550899 [doi] PST - ppublish SO - J Environ Sci Health B. 2007 Sep-Oct;42(7):767-73. doi: 10.1080/03601230701550899.