PMID- 18257309
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20100615
LR  - 20161018
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 25
IP  - 6
DP  - 2007 Nov
TI  - [Determination of seven nitrobenzene compounds in water samples by single-drop 
      microextraction with capillary gas chromatography].
PG  - 876-80
AB  - A method suitable for the extraction of nitrobenzene, nitrotoluenes and 
      nitrochlorobenzenes from water samples using single-drop microextraction with 
      capillary gas chromatography is presented. Parameters, such as organic solvents, 
      drop volume of organics, agitation, immerge depth of needle point, aqueous sample 
      volume, exposure time and temperature were controlled and optimized. The 
      developed protocol was found to yield a linear calibration curve in a 
      concentration range from 0.8 to 32 microg/L for nitrobenzene and nitrotoluenes 
      and a range from 0.04 to 3.2 microg/L for nitrochlorobenzenes (r2 > 0.999). The 
      limits of detection were found to be in the range between 0.01 and 0.3 microg/L. 
      The relative standard deviations (RSDs) and relative recoveries (n = 5) from tap 
      water fortified samples were 3.1% -7.9%, and 101% - 105%, and from waste water 
      fortified samples were 3.3% - 7.9%, and 92.5% - 97.0%, respectively. The 
      single-drop microextraction is proved to be a environmental friendly, sensitive, 
      fast and simple tool for the preconcentration of trace nitrobenzene, 
      nitrotoluenes and nitrochlorobenzenes from water samples.
FAU - Mu, Yingfeng
AU  - Mu Y
AD  - Nanjing Environment Monitoring Center, Nanjing 210013, China. myf125@163.com
FAU - Yang, Lili
AU  - Yang L
FAU - Hu, Enyu
AU  - Hu E
FAU - Ji, Ying
AU  - Ji Y
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
EDAT- 2008/02/09 09:00
MHDA- 2008/02/09 09:01
CRDT- 2008/02/09 09:00
PHST- 2008/02/09 09:00 [pubmed]
PHST- 2008/02/09 09:01 [medline]
PHST- 2008/02/09 09:00 [entrez]
PST - ppublish
SO  - Se Pu. 2007 Nov;25(6):876-80.