PMID- 18257313
OWN - NLM
STAT- MEDLINE
DCOM- 20100615
LR  - 20171116
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 25
IP  - 6
DP  - 2007 Nov
TI  - [Determination of azoxystrobin residues in fruits and vegetables by gas 
      chromatography/mass spectrometry with solid-phase extraction].
PG  - 898-901
AB  - A method was developed for the determination of azoxystrobin residues in fruits 
      and vegetables by gas chromatography/mass spectrometry (GC/MS). Azoxystrobin 
      residues were extracted with ethyl acetate-cyclohexane (1 : 1, v/v) by 
      ultrasonication and then they were cleaned up on a silica solid-phase extraction 
      (SPE) column to obtain an extract suitable for analysis by GC/MS in the selective 
      ion monitoring (SIM) mode (the selected ion: m/z 344, 372, 388 and 403). The 
      calibration curves were linear between area and concentration of azoxystrobin 
      from 0.01 to 1.0 mg/kg with the correlation coefficient greater than 0.99. The 
      average recoveries from spiked fruit and vegetable matrixes at three 
      concentrations of 0.01, 0.1, 1.0 mg/kg ranged from 85.2% to 98.2% with relative 
      standard deviation less than 21.5%. The limit of detection was 0.01 mg/kg and the 
      limit of quantity was 0.05 mg/kg in fruit and vegetable matrixes, respectively.
FAU - Bo, Haibo
AU  - Bo H
AD  - Qinghai Entry-Exit Inspection and Quarantine Bureau, Xining 810000, China. 
      bohb1212@163.com
LA  - chi
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Methacrylates)
RN  - 0 (Pyrimidines)
RN  - 0 (Strobilurins)
RN  - NYH7Y08IPM (azoxystrobin)
SB  - IM
MH  - Fruit/*chemistry
MH  - Gas Chromatography-Mass Spectrometry/*methods
MH  - Limit of Detection
MH  - Methacrylates/*analysis
MH  - Pyrimidines/*analysis
MH  - Solid Phase Extraction/*methods
MH  - Strobilurins
MH  - Vegetables/*chemistry
EDAT- 2008/02/09 09:00
MHDA- 2010/06/16 06:00
CRDT- 2008/02/09 09:00
PHST- 2008/02/09 09:00 [pubmed]
PHST- 2010/06/16 06:00 [medline]
PHST- 2008/02/09 09:00 [entrez]
PST - ppublish
SO  - Se Pu. 2007 Nov;25(6):898-901.