PMID- 18314265
OWN - NLM
STAT- MEDLINE
DCOM- 20090122
LR  - 20121115
IS  - 0304-3894 (Print)
IS  - 0304-3894 (Linking)
VI  - 158
IP  - 1
DP  - 2008 Oct 1
TI  - A solid phase extraction procedure for Fe3+, Cu2+ and Zn2+ ions on 
      2-phenyl-1H-benzo[d] imidazole loaded on Triton X-100-coated polyvinyl chloride.
PG  - 131-6
LID - 10.1016/j.jhazmat.2008.01.037 [doi]
AB  - A new and efficient solid phase extraction method is described for the 
      preconcentration of trace heavy metal ions. The method is based on the adsorption 
      of Fe(3+), Cu(2+) and Zn(2+) on 2-phenyl-1H-benzo[d] imidazole (PHBI) loaded on 
      Triton X-100-coated polyvinyl chloride (PVC). The influences of the analytical 
      parameters including pH and sample volume were investigated. Common coexisting 
      ions did not interfere on the separation and determination of analytes under 
      study. The adsorbed analytes were desorbed by using 5 mL of 4 mol L(-1) nitric 
      acid. The preconcentration factor is 90. The detection limits (3 sigma) were in 
      the range of 0.95-1 microg L(-1). The sorbent exhibited excellent stability and 
      its sorption capacity under optimum conditions has been found to be more than 2.7 
      mg of ions per gram of sorbent. The recoveries of analytes were generally higher 
      than 95%. The relative standard deviations (R.S.D.s) were generally lower than 
      4%. The method has been successfully applied to some real samples.
FAU - Ghaedi, Mehrorang
AU  - Ghaedi M
AD  - Chemistry Department, Yasouj University, Yasouj 75914-353, Iran. 
      m_ghaedi@mail.yu.ac.ir
FAU - Niknam, Khodabakhsh
AU  - Niknam K
FAU - Shokrollahi, Ardeshir
AU  - Shokrollahi A
FAU - Niknam, Ebrahim
AU  - Niknam E
FAU - Ghaedi, Hamed
AU  - Ghaedi H
FAU - Soylak, Mustafa
AU  - Soylak M
LA  - eng
PT  - Journal Article
DEP - 20080119
PL  - Netherlands
TA  - J Hazard Mater
JT  - Journal of hazardous materials
JID - 9422688
RN  - 0 (Benzimidazoles)
RN  - 0 (Ions)
RN  - 0 (Metals, Heavy)
RN  - 0 (Surface-Active Agents)
RN  - 9002-86-2 (Polyvinyl Chloride)
RN  - 9002-93-1 (Octoxynol)
RN  - CB9ZJ140SB (2-phenylbenzimidazole)
SB  - IM
MH  - Benzimidazoles/*chemistry
MH  - Equipment Reuse
MH  - Hydrogen-Ion Concentration
MH  - Ions/chemistry
MH  - Metals, Heavy/*chemistry
MH  - Octoxynol/*chemistry
MH  - Polyvinyl Chloride/*chemistry
MH  - Reproducibility of Results
MH  - Solid Phase Extraction/*methods
MH  - Surface-Active Agents/chemistry
EDAT- 2008/03/04 09:00
MHDA- 2009/01/23 09:00
CRDT- 2008/03/04 09:00
PHST- 2007/11/29 00:00 [received]
PHST- 2008/01/13 00:00 [revised]
PHST- 2008/01/14 00:00 [accepted]
PHST- 2008/03/04 09:00 [pubmed]
PHST- 2009/01/23 09:00 [medline]
PHST- 2008/03/04 09:00 [entrez]
AID - S0304-3894(08)00112-X [pii]
AID - 10.1016/j.jhazmat.2008.01.037 [doi]
PST - ppublish
SO  - J Hazard Mater. 2008 Oct 1;158(1):131-6. doi: 10.1016/j.jhazmat.2008.01.037. Epub 
      2008 Jan 19.