PMID- 18371921
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20080808
LR  - 20080328
IS  - 1873-3573 (Electronic)
IS  - 0039-9140 (Linking)
VI  - 75
IP  - 2
DP  - 2008 Apr 15
TI  - Organotin speciation in textile and plastics by microwave-assisted extraction 
      HPLC-ESI-MS.
PG  - 556-63
LID - 10.1016/j.talanta.2007.11.050 [doi]
AB  - The HPLC coupled with electrospray ionization mass spectrometry (ESI-MS) was 
      applied for the determination of tributyltin chloride (TBT), triphenyltin 
      chloride (TPhT), triethyltin chloride (TET) in textile and plastic samples. The 
      separation was performed in the isocratic mode on ion exchange SCX column with a 
      mobile phase containing methanol-ammonium acetate (50 mmol l(-1))-acetic acid 
      (90/9.98/0.02, v/v/v). Sensitive detection of three organotin compounds by ESI-MS 
      was performed on the basis of multiple reaction monitoring (MRM) mode. Limits of 
      detection were 0.4, 20, 4 ng ml(-1) for TBT, TPhT, and TET, respectively. 
      Microwave-assisted extraction (MAE) of organotin compounds was finished in 60% 
      (v/v) methanol aqueous solution. Under the experimental conditions used, 
      recoveries of three organotin compounds obtained for spiked textile and plastic 
      samples are in the range of 55-95% and the R.S.D.s are 3-9%.
FAU - Wang, Xiupin
AU  - Wang X
AD  - College of Chemistry, Jilin University, Changchun 130012, PR China.
FAU - Jin, Haiyan
AU  - Jin H
FAU - Ding, Lan
AU  - Ding L
FAU - Zhang, Huarong
AU  - Zhang H
FAU - Zhang, Hanqi
AU  - Zhang H
FAU - Qu, Chenling
AU  - Qu C
FAU - Yu, Aimin
AU  - Yu A
LA  - eng
PT  - Journal Article
DEP - 20071128
PL  - Netherlands
TA  - Talanta
JT  - Talanta
JID - 2984816R
EDAT- 2008/03/29 09:00
MHDA- 2008/03/29 09:01
CRDT- 2008/03/29 09:00
PHST- 2007/08/29 00:00 [received]
PHST- 2007/11/19 00:00 [revised]
PHST- 2007/11/19 00:00 [accepted]
PHST- 2008/03/29 09:00 [pubmed]
PHST- 2008/03/29 09:01 [medline]
PHST- 2008/03/29 09:00 [entrez]
AID - S0039-9140(07)00830-2 [pii]
AID - 10.1016/j.talanta.2007.11.050 [doi]
PST - ppublish
SO  - Talanta. 2008 Apr 15;75(2):556-63. doi: 10.1016/j.talanta.2007.11.050. Epub 2007 
      Nov 28.