PMID- 18576219
OWN - NLM
STAT- MEDLINE
DCOM- 20080908
LR  - 20191210
IS  - 1532-4109 (Electronic)
IS  - 0360-1234 (Linking)
VI  - 43
IP  - 5
DP  - 2008 Jun
TI  - Evaluation of pressurized liquid extraction for the analysis of four pesticides 
      in unpolished rice.
PG  - 390-4
LID - 10.1080/10934520701795608 [doi]
AB  - The aim of to evaluate efficiency of this study was extraction pressurized liquid 
      extraction (PLE) for the analysis of four pesticides, fthalide, etofenprox, 
      fenitrothion, and isoprothiolane, in unpolished rice by comparing with 
      homogenization as a reference technique. The concentrations of four selected 
      pesticides obtained by PLE with acetonitrile at 130 degrees C for 10 min x 2 
      cycles were comparable to those by homogenization with water-soaking. The 
      repeatability of the analysis, represented as relative standard deviations 
      (RSDs), were 1.4-3.6% (n = 3) for PLE at 130 degrees C and 1.2-3.8% (n = 3) for 
      homogenization with water-soaking. Recovery yields of surrogates were 75-88% and 
      87-109% for PLE at 130 degrees C and homogenization with water-soaking, 
      respectively, and these were satisfactory according to the method of positive 
      list. This study suggested that PLE can be applied for the analysis of selected 
      four pesticides in unpolished rice as well as homogenization with water-soaking.
FAU - Otake, Takamitsu
AU  - Otake T
AD  - National Metrology Institute of Japan (NMIJ), National Institute of Advanced 
      Industrial Science and Technology (AIST), Ibaraki, Japan. t-ootake@aist.go.jp
FAU - Aoyagi, Yoshie
AU  - Aoyagi Y
FAU - Matsuo, Mayumi
AU  - Matsuo M
FAU - Itoh, Nobuyasu
AU  - Itoh N
FAU - Yarita, Takashi
AU  - Yarita T
LA  - eng
PT  - Evaluation Study
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
PL  - England
TA  - J Environ Sci Health B
JT  - Journal of environmental science and health. Part. B, Pesticides, food 
      contaminants, and agricultural wastes
JID - 7607167
RN  - 0 (Pesticides)
RN  - 0 (Soil Pollutants)
RN  - 059QF0KO0R (Water)
SB  - IM
MH  - Chromatography, Gas
MH  - *Clinical Laboratory Techniques
MH  - Mass Spectrometry
MH  - Oryza/*chemistry
MH  - Pesticides/*analysis
MH  - Reference Standards
MH  - Reproducibility of Results
MH  - Soil Pollutants/*analysis
MH  - Solubility
MH  - Temperature
MH  - Water/*chemistry
EDAT- 2008/06/26 09:00
MHDA- 2008/09/09 09:00
CRDT- 2008/06/26 09:00
PHST- 2008/06/26 09:00 [pubmed]
PHST- 2008/09/09 09:00 [medline]
PHST- 2008/06/26 09:00 [entrez]
AID - 794426922 [pii]
AID - 10.1080/10934520701795608 [doi]
PST - ppublish
SO  - J Environ Sci Health B. 2008 Jun;43(5):390-4. doi: 10.1080/10934520701795608.