PMID- 18724672
OWN - NLM
STAT- MEDLINE
DCOM- 20100617
LR  - 20161018
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 26
IP  - 3
DP  - 2008 May
TI  - [Determination of melamine residue in feeds by ultra performance liquid 
      chromatography coupled with electrospray tandem mass spectrometry].
PG  - 339-42
AB  - A method for fast determination melamine residue in feeds was established. An 
      ultra performance liquid chromatography coupled with electrospray ionization 
      quadrupole tandem mass spectrometry (UPLC-ESI-MS/MS) was used. The residue was 
      quantified with multiple reaction monitoring (MRM) mode. The method was validated 
      and good results were obtained with respect to precision, repeatability and 
      spiked recovery. The limit of detection was 10 microg/kg for melamine, and the 
      linear range was from 10 to 5 000 1g/kg. The average recoveries were between 83% 
      and 94% in the spiked range of 10 - 100 microg/kg, and the relative standard 
      deviations (RSDs) were between 4.2% and 6.5%. The method has good repeatability 
      and high sensitivity, and can be applied for the determination of melamine 
      residue in feeds.
FAU - Cai, Qinren
AU  - Cai Q
AD  - Technical Center of Zhuhai Entry-Exit Inspection and Quarantine Bureau, Zhuhai 
      519015, China. mr.cai@vip.163.com
FAU - Ouyang, Yingyu
AU  - Ouyang Y
FAU - Qian, Zhenjie
AU  - Qian Z
FAU - Peng, Yufen
AU  - Peng Y
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Triazines)
RN  - N3GP2YSD88 (melamine)
SB  - IM
MH  - Animal Feed/*analysis/standards
MH  - Chromatography, High Pressure Liquid/*methods
MH  - Food Analysis/*methods
MH  - Food Contamination/*analysis
MH  - Hydrogen-Ion Concentration
MH  - Limit of Detection
MH  - Linear Models
MH  - Quality Control
MH  - Reproducibility of Results
MH  - Spectrometry, Mass, Electrospray Ionization/*methods
MH  - Time Factors
MH  - Triazines/*analysis
EDAT- 2008/08/30 09:00
MHDA- 2010/06/18 06:00
CRDT- 2008/08/30 09:00
PHST- 2008/08/30 09:00 [pubmed]
PHST- 2010/06/18 06:00 [medline]
PHST- 2008/08/30 09:00 [entrez]
PST - ppublish
SO  - Se Pu. 2008 May;26(3):339-42.