PMID- 18793487 OWN - NLM STAT- MEDLINE DCOM- 20081118 LR - 20131121 IS - 1431-9276 (Print) IS - 1431-9276 (Linking) VI - 14 IP - 5 DP - 2008 Oct TI - High-resolution transmission electron microscopy study of nanostructured hydroxyapatite. PG - 433-8 LID - 10.1017/S1431927608080744 [doi] AB - Crystalline properties of synthetic nanostructured hydroxyapatite (n-HA) were studied using high-resolution transmission electron microscopy. The focal-series-restoration technique, obtaining exit-plane wavefunction and spherical aberration-corrected images, was successfully applied for the first time in this electron-beam-susceptible material. Multislice simulations and energy dispersive X-ray spectroscopy were also employed to determine unequivocally that n-HA particles of different size preserve stoichiometric HA-like crystal structure. n-HA particles with sizes of twice the HA lattice parameter were found. These results can be used to optimize n-HA sinterization parameters to improve bioactivity. FAU - Biggemann, Daniel AU - Biggemann D AD - Brazilian Synchrotron Light Laboratory, Caixa Postal 6192, Campinas-SP 13083-970, Brazil. FAU - da Silva, Marcelo H Prado AU - da Silva MH FAU - Rossi, Alexandre M AU - Rossi AM FAU - Ramirez, Antonio J AU - Ramirez AJ LA - eng PT - Journal Article PT - Research Support, Non-U.S. Gov't PL - England TA - Microsc Microanal JT - Microscopy and microanalysis : the official journal of Microscopy Society of America, Microbeam Analysis Society, Microscopical Society of Canada JID - 9712707 RN - 91D9GV0Z28 (Durapatite) SB - IM MH - Durapatite/*chemistry MH - Microscopy, Electron, Transmission MH - Nanostructures/*chemistry MH - Spectrum Analysis EDAT- 2008/09/17 09:00 MHDA- 2008/11/19 09:00 CRDT- 2008/09/17 09:00 PHST- 2008/09/17 09:00 [pubmed] PHST- 2008/11/19 09:00 [medline] PHST- 2008/09/17 09:00 [entrez] AID - S1431927608080744 [pii] AID - 10.1017/S1431927608080744 [doi] PST - ppublish SO - Microsc Microanal. 2008 Oct;14(5):433-8. doi: 10.1017/S1431927608080744.