PMID- 18966786
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20121002
LR  - 20190729
IS  - 0039-9140 (Print)
IS  - 0039-9140 (Linking)
VI  - 44
IP  - 4
DP  - 1997 Apr
TI  - Gas chromatography-mass spectrometric determination of fthalide and heptachlor 
      epoxide in environmental samples.
PG  - 649-56
AB  - Methods were developed to determine traces of 4,5,6,7-tetrachlorophthalide 
      (fthalide) and 
      1,4,5,6,7,8,8-heptachloro-2,3-epoxy-2,3,3a,7a-tetrahydro-4,7-methanoindene 
      (heptachlor epoxide) in environmental samples such as river water, sediment and 
      fish. The samples were cleaned up by using convenient disk type solid phase 
      extractors and cartridges and analyzed by GC/MS with selected ion monitoring. 
      Fthalide and heptachlor epoxide in water samples could be determined in the range 
      0.1-0.3 ng ml(-1) with relative standard deviations (RSDs) of 1.0-4.8%. The 
      estimated detection limits were 0.020-0.031 ng ml(-1), 5.1-7.3 ng g(-1) and 
      2.7-4.2 ng g(-1) in water, sediment and fish samples, respectively. The 
      recoveries were 96-103, 99-101, 66-85 and 67-77% with RSDs of 4.3-10.2, 2.4-2.5, 
      4.6-5.2 and 2.1-3.8% in river water, sea water, sediment and fish samples, 
      respectively.
FAU - Okumura, T
AU  - Okumura T
AD  - Environmental Pollution Control Center, 1-3-62, Nakamichi, Higashinari-ku, Osaka 
      City 537, Japan.
FAU - Nishikawa, Y
AU  - Nishikawa Y
FAU - Yamamoto, H
AU  - Yamamoto H
FAU - Konishi, H
AU  - Konishi H
LA  - eng
PT  - Journal Article
PL  - Netherlands
TA  - Talanta
JT  - Talanta
JID - 2984816R
EDAT- 1997/04/01 00:00
MHDA- 1997/04/01 00:01
CRDT- 1997/04/01 00:00
PHST- 1996/08/30 00:00 [accepted]
PHST- 1997/04/01 00:00 [pubmed]
PHST- 1997/04/01 00:01 [medline]
PHST- 1997/04/01 00:00 [entrez]
AID - S0039-9140(96)02097-8 [pii]
AID - 10.1016/s0039-9140(96)02097-8 [doi]
PST - ppublish
SO  - Talanta. 1997 Apr;44(4):649-56. doi: 10.1016/s0039-9140(96)02097-8.