PMID- 19233552
OWN - NLM
STAT- MEDLINE
DCOM- 20091211
LR  - 20191210
IS  - 1873-3336 (Electronic)
IS  - 0304-3894 (Linking)
VI  - 167
IP  - 1-3
DP  - 2009 Aug 15
TI  - Molecularly imprinted solid-phase extraction combined with high performance 
      liquid chromatography for analysis of phenolic compounds from environmental water 
      samples.
PG  - 282-8
LID - 10.1016/j.jhazmat.2008.12.115 [doi]
AB  - The molecularly imprinted bulk polymer with 2,4,6-trichlorophenol (2,4,6-TCP) as 
      the template molecule and methylacrylic acid (MAA), ethylene glycol 
      dimethacrylate (EGDMA) as functional monomer and the crosslinker, respectively, 
      has been prepared and applied to the molecularly imprinted solid-phase extraction 
      (MISPE) procedure for selective preconcentration of phenolic compounds from 
      environmental water samples. Various parameters affecting the extraction 
      efficiency of the polymer have been evaluated to optimize the selective 
      preconcentration of the phenolic compounds from aqueous samples. The 
      characteristics of the MISPE method were validated by HPLC. The recoveries ranged 
      between 90% and 98% (RSD: 0.9-2.3%, n=3) for tap water, between 85% and 105% 
      (RSD: 2.6-4.9%, n=3) for river water, between 78% and 98% (RSD: 2.6-5.4%, n=3) 
      for sewage water fortified with 0.4 mg L(-1) of phenol, 4-chlorophenol (4-CP), 
      2,4-dichlorophenol (2,4-DCP), pentachlorophenol (PCP). It was demonstrated that 
      this MISPE-HPLC method could be applied to direct preconcentration and 
      determination of phenolic compounds in environmental water samples.
FAU - Feng, Qin-Zhong
AU  - Feng QZ
AD  - State Key Laboratory of Environmental Chemistry and Ecotoxicology, Research 
      Center for Eco-Environmental Sciences, Chinese Academy of Sciences, Beijing, 
      China.
FAU - Zhao, Li-Xia
AU  - Zhao LX
FAU - Yan, Wei
AU  - Yan W
FAU - Lin, Jin-Ming
AU  - Lin JM
FAU - Zheng, Zhi-Xia
AU  - Zheng ZX
LA  - eng
PT  - Evaluation Study
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
DEP - 20081231
PL  - Netherlands
TA  - J Hazard Mater
JT  - Journal of hazardous materials
JID - 9422688
RN  - 0 (Chlorophenols)
RN  - 0 (Industrial Waste)
RN  - 0 (Phenols)
RN  - 0 (Polymers)
RN  - 0 (Water Pollutants, Chemical)
RN  - MHS8C5BAUZ (2,4,6-trichlorophenol)
SB  - IM
MH  - Chlorophenols
MH  - Chromatography, High Pressure Liquid
MH  - Industrial Waste/*prevention & control
MH  - *Molecular Imprinting
MH  - Phenols/*analysis/isolation & purification
MH  - Polymers
MH  - Solid Phase Extraction/*methods
MH  - Water Pollutants, Chemical/*analysis/isolation & purification
EDAT- 2009/02/24 09:00
MHDA- 2009/12/16 06:00
CRDT- 2009/02/24 09:00
PHST- 2008/09/10 00:00 [received]
PHST- 2008/11/25 00:00 [revised]
PHST- 2008/12/24 00:00 [accepted]
PHST- 2009/02/24 09:00 [entrez]
PHST- 2009/02/24 09:00 [pubmed]
PHST- 2009/12/16 06:00 [medline]
AID - S0304-3894(08)01965-1 [pii]
AID - 10.1016/j.jhazmat.2008.12.115 [doi]
PST - ppublish
SO  - J Hazard Mater. 2009 Aug 15;167(1-3):282-8. doi: 10.1016/j.jhazmat.2008.12.115. 
      Epub 2008 Dec 31.