PMID- 19436151
OWN - NLM
STAT- MEDLINE
DCOM- 20090818
LR  - 20191111
IS  - 1882-1006 (Electronic)
IS  - 0015-6426 (Linking)
VI  - 50
IP  - 2
DP  - 2009 Apr
TI  - [Determination of bicozamycin in livestock products and seafoods by liquid 
      chromatography-tandem mass spectrometry].
PG  - 52-7
AB  - A novel liquid chromatography-tandem mass spectrometry (LC-MS/MS) method was 
      developed for trace residue determination of bicozamycin (BZM) in livestock 
      products and seafoods. BZM was extracted from a sample with acetonitrile-water (4 
      : 1), followed by a two-stage SPE enrichment and cleanup. The first stage 
      involved a styrene-divinylbenzene copolymer cartridge (GL-Pak PLS-2), and the 
      second stage involved a divinylbenzene-N-vinylpyrrolidone copolymer cartridge 
      (Oasis HLB). The LC separation was performed on a C18 column using 0.01% formic 
      acid-methanol (8 : 2) as the mobile phase and MS detection with negative ion 
      electrospray ionization. The mean recoveries from swine muscle, liver, 
      yellowtail, and milk fortified at the minimum residue limit (MRL) levels and 0.01 
      microg/g were >70%, and the relative standard deviations (RSDs) were <20%. Limits 
      of quantitation (LOQs) ranged from 0.002 to 0.005 microg/g.
FAU - Fujita, Kazuhiro
AU  - Fujita K
AD  - Japan Food Research Laboratories, Ibaraki-shi, Osaka 5670085, Japan.
FAU - Nakanishi, Akiko
AU  - Nakanishi A
FAU - Ishihara, Michiyo
AU  - Ishihara M
FAU - Ito, Hironobu
AU  - Ito H
FAU - Nakamura, Munetomo
AU  - Nakamura M
FAU - Watai, Masatoshi
AU  - Watai M
FAU - Taniguchi, Makoto
AU  - Taniguchi M
FAU - Murayama, Mitsunori
AU  - Murayama M
LA  - jpn
PT  - Journal Article
PL  - Japan
TA  - Shokuhin Eiseigaku Zasshi
JT  - Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan
JID - 0142214
RN  - 0 (Anti-Bacterial Agents)
RN  - 0 (Bridged Bicyclo Compounds, Heterocyclic)
RN  - J03U9E2P82 (bicozamycin)
SB  - IM
MH  - Animals
MH  - *Animals, Domestic
MH  - Anti-Bacterial Agents/*analysis
MH  - Bridged Bicyclo Compounds, Heterocyclic/analysis
MH  - Chromatography, Liquid/*methods
MH  - Fishes
MH  - Seafood/*analysis
MH  - Swine
MH  - Tandem Mass Spectrometry/*methods
EDAT- 2009/05/14 09:00
MHDA- 2009/08/19 09:00
CRDT- 2009/05/14 09:00
PHST- 2009/05/14 09:00 [entrez]
PHST- 2009/05/14 09:00 [pubmed]
PHST- 2009/08/19 09:00 [medline]
AID - JST.JSTAGE/shokueishi/50.52 [pii]
AID - 10.3358/shokueishi.50.52 [doi]
PST - ppublish
SO  - Shokuhin Eiseigaku Zasshi. 2009 Apr;50(2):52-7. doi: 10.3358/shokueishi.50.52.
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