PMID- 19938491
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20101005
LR  - 20161018
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 27
IP  - 4
DP  - 2009 Jul
TI  - [Determination of 107 pesticide residues in vegetables using off-line dispersive 
      solid-phase extraction and gas chromatography-tandem mass spectrometry].
PG  - 391-400
AB  - A screening method was developed for the determination of 107 pesticide residues 
      in vegetables using off-line dispersive solid-phase extraction (DSPE) and gas 
      chromatography-tandem mass spectrometry (GC-MS/MS). The pesticides interested 
      were extracted from the samples with acetonitrile (saturated by n-hexane) 
      containing 1% acetic acid and simultaneously separated by liquid-liquid 
      partitioning with adding anhydrous magnesium sulfate plus sodium acetate 
      following by a simple cleanup step known as dispersive solid-phase extraction. 
      The extracts were determined by GC-MS/MS using external standard method. The 
      method was reliable and stable that the recoveries of almost all pesticides were 
      in the range from 60% to 130% at the spiked level of 10 microg/kg into four 
      vegetable matrixes (garlic, green bean, radish 8 and spinach) and the relative 
      standard deviations (RSDs) were all not more than 15.3%. The linearity of the 
      method was good between 0.05 mg/L and 1 mg/L, and all limits of quantification 
      (LOQs) less than 10 microg/kg. The method is selective with no interference, 
      especially in the complicated garlic matrix.
FAU - Shen, Weijian
AU  - Shen W
AD  - Food Laboratory of Jiangsu Entry-Exit Inspection and Quarantine Bureau, Nanjing, 
      China. swj9722418@yahoo.com.cn
FAU - Yu, Keyao
AU  - Yu K
FAU - Gui, Qianwen
AU  - Gui Q
FAU - Jiang, Yuan
AU  - Jiang Y
FAU - Zhao, Zengyun
AU  - Zhao Z
FAU - Shen, Chongyu
AU  - Shen C
FAU - Wu, Bin
AU  - Wu B
FAU - Chu, Xiaogang
AU  - Chu X
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
EDAT- 2009/11/27 06:00
MHDA- 2009/11/27 06:01
CRDT- 2009/11/27 06:00
PHST- 2009/11/27 06:00 [entrez]
PHST- 2009/11/27 06:00 [pubmed]
PHST- 2009/11/27 06:01 [medline]
PST - ppublish
SO  - Se Pu. 2009 Jul;27(4):391-400.