PMID- 19938513
OWN - NLM
STAT- MEDLINE
DCOM- 20101005
LR  - 20161018
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 27
IP  - 4
DP  - 2009 Jul
TI  - [Determination of five biogenic amines in source water by ion chromatography].
PG  - 505-8
AB  - An ion chromatographic (IC) method was developed for the separation of five 
      biogenic amines (BAs), including putrescine, cadaverine, histamine, spermidine 
      and spermine, in source water. The sample was separated on a TSK-GEL SuperIC 
      cation exchange column (150 mm x 4.6 mm) after filtering treatment by 0.45 microm 
      inorganic membrane. Methanesulfonic acid was used as eluent for concentration 
      gradient elution at the rate of 1.0 mL/min. The injection volume was 100 microL 
      and the BAs were detected by a non-suppressed conductivity detector. The result 
      showed that the baseline separation was obtained for the 5 kinds of BAs. The 
      linear relationships between the concentration and the peak area were obtained in 
      the concentration range of 1.0 - 30.0 mg/L. The relative standard deviations 
      (RSDs) of retention time and peak area were no more than 0.02% and 2.08%, 
      respectively. The recoveries were from 96.0% to 107.0%. The method is simple, 
      rapid, highly sensitive and with good repeatability. It could be used for the 
      determination the BAs in the source water.
FAU - Zhao, Xinying
AU  - Zhao X
AD  - Beijing Center for Physical and Chemical Analysis, Beijing, China. 
      zhaoxinying_123@sina.com
FAU - Jiao, Xia
AU  - Jiao X
FAU - Xia, Min
AU  - Xia M
FAU - Liu, Qing
AU  - Liu Q
FAU - Zhang, Jinghua
AU  - Zhang J
LA  - chi
PT  - English Abstract
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Biogenic Amines)
RN  - 0 (Water Pollutants, Chemical)
RN  - 2FZ7Y3VOQX (Spermine)
RN  - 820484N8I3 (Histamine)
RN  - L90BEN6OLL (Cadaverine)
RN  - U87FK77H25 (Spermidine)
RN  - V10TVZ52E4 (Putrescine)
SB  - IM
MH  - Biogenic Amines/*analysis
MH  - Cadaverine/analysis
MH  - Chromatography, Ion Exchange/*methods
MH  - Fresh Water/*analysis
MH  - Histamine/analysis
MH  - Putrescine/analysis
MH  - Spermidine/analysis
MH  - Spermine/analysis
MH  - Water Pollutants, Chemical/*analysis
EDAT- 2009/11/27 06:00
MHDA- 2010/10/06 06:00
CRDT- 2009/11/27 06:00
PHST- 2009/11/27 06:00 [entrez]
PHST- 2009/11/27 06:00 [pubmed]
PHST- 2010/10/06 06:00 [medline]
PST - ppublish
SO  - Se Pu. 2009 Jul;27(4):505-8.