PMID- 19938515
OWN - NLM
STAT- MEDLINE
DCOM- 20101005
LR  - 20161018
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 27
IP  - 4
DP  - 2009 Jul
TI  - [Rapid determination of melamine in eggs by high performance liquid 
      chromatography].
PG  - 513-5
AB  - A rapid method for the determination of melamine in eggs was established using 
      high performance liquid chromatography (HPLC). The melamine in a test sample was 
      extracted with ultrasonic in 1% trichloroacetic acid for 10 min, and then 
      purified with precipitation, centrifugation and filtration, at last tested by 
      HPLC system. The total time of HPLC analysis for each sample was only 10 min. The 
      linear range was from 0.05 to 20.0 mg/L as the linear correlation coefficient was 
      0. 999 9. The limit of quantification was 0. 10 mg/kg (S/N > 10). The average 
      recoveries were between 94.2% and 107% in the spiked range of 1.0 - 6.0 mg/kg in 
      eggs. The relative standard deviations (RSDs) of parallel determination were 
      between 1.53% and 2.06% (n = 6). This method is simple, fast, sensitive and 
      suitable for the determination of melamine in eggs.
FAU - Tang, Tao
AU  - Tang T
AD  - Dalian Elite Analytical Instruments Co., Ltd., Dalian, China.
FAU - Li, Shuanghua
AU  - Li S
FAU - Liu, Fan
AU  - Liu F
FAU - Yu, Shuxin
AU  - Yu S
FAU - Li, Tong
AU  - Li T
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Triazines)
RN  - N3GP2YSD88 (melamine)
SB  - IM
MH  - Animals
MH  - Chickens
MH  - Chromatography, High Pressure Liquid/*methods
MH  - Eggs/*analysis
MH  - Food Contamination/analysis
MH  - Triazines/*analysis
EDAT- 2009/11/27 06:00
MHDA- 2010/10/06 06:00
CRDT- 2009/11/27 06:00
PHST- 2009/11/27 06:00 [entrez]
PHST- 2009/11/27 06:00 [pubmed]
PHST- 2010/10/06 06:00 [medline]
PST - ppublish
SO  - Se Pu. 2009 Jul;27(4):513-5.