PMID- 20352934
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20131212
LR  - 20161018
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 27
IP  - 6
DP  - 2009 Nov
TI  - [Dispersive liquid-liquid microextraction coupled with high performance liquid 
      chromatography for the determination of polynuclear aromatic hydrocarbons in 
      environmental water samples].
PG  - 799-803
AB  - A simple, rapid and effective method, the dispersive liquid-liquid 
      microextraction coupled with high performance liquid chromatography-fluorescence 
      detection (DLLME-HPLCFLD), has been developed for the extraction and 
      determination of polynuclear aromatic hydrocarbons (PAHs) in environmental water 
      samples. The factors relevant to the microextraction efficiency, such as type and 
      volume of dispersion agent and extraction solvents and the extraction time were 
      investigated and optimized. Under the optimized extraction conditions, the 
      reliability of the proposed method was evaluated. The linear response of this 
      method was in the range of 0.01-10 microg/L (r > or = 0.9913), the relative 
      standard deviations (RSDs) of peak area for 0.05 microg/L PAHs were in the range 
      of 2.3%-4.7% (n = 6). At room temperature, the method exhibited excellent 
      enrichment factors and good recoveries, 674-1032 and 67.4%-103.2% respectively. 
      The detection limits (S/N = 3) were in the range of 0. 000 3 - 0. 002 pg/L. The 
      developed method was applied to the determination of 15 PAHs in the water from 
      Aojiang river, the average recoveries were 79.5% -92.3% with RSD of 4.3%-6.7% (n 
      = 5). The developed method is suitable for the analysis of trace PAHs in 
      environmental water samples.
FAU - Zhang, Jianhua
AU  - Zhang J
AD  - Ministry of Education Key Laboratory of Analysis and Detection Technology for 
      Food Safety, Department of Chemistry, Fuzhou University, Fuzhou 350002, China.
FAU - Huang, Ying
AU  - Huang Y
FAU - Chen, Xiaoqiu
AU  - Chen X
FAU - Chen, Jinhua
AU  - Chen J
FAU - Li, Hui
AU  - Li H
FAU - Chen, Guonan
AU  - Chen G
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
EDAT- 2010/04/01 06:00
MHDA- 2010/04/01 06:01
CRDT- 2010/04/01 06:00
PHST- 2010/04/01 06:00 [entrez]
PHST- 2010/04/01 06:00 [pubmed]
PHST- 2010/04/01 06:01 [medline]
PST - ppublish
SO  - Se Pu. 2009 Nov;27(6):799-803.