PMID- 20352944
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20131212
LR  - 20161018
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 27
IP  - 6
DP  - 2009 Nov
TI  - [Determination of fosetyl-aluminium by ion-pair reversed phase-high performance 
      liquid chromatography with evaporative light scattering detection].
PG  - 849-51
AB  - Ion-pair reversed phase-high performance liquid chromatography (RP-HPLC) with 
      evaporative light scattering detection (ELSD) has been established for the 
      analysis of fosetyl-aluminium and relevant impurities in technical or formulated 
      substance. The method was achieved on a Symmetry Shield RP18 column by using 
      n-butylamine as ion-pairing agent. The mobile phase was methanol-redistilled 
      water containing 0.5% n-butylamine which was adjusted pH 5.0 with acetic acid 
      (8:92, v/v) and the flow rate was set at 0.8 mL/min. The active ingredient 
      fosetyl-aluminium was successfully separated from relevant impurities under the 
      conditions. The calibration curve was linear in the range of 100-1200 mg/L. The 
      average recoveries of two fortification levels (100 mg/L and 1000 mg/L) were 
      100.58% and 99.53%, and the relative standard deviations (RSDs) were 0.62% and 
      0.49%, respectively. The method is rapid, simple and accurate which provides 
      another new and reliable means for the analysis of fosetyl-aluminium in its 
      technical or formulated substance.
FAU - Fan, Zhixian
AU  - Fan Z
AD  - College of Chemical Engineering, Qingdao University of Science and Technology, 
      Qingdao 266042, China. fanzx@qust.edu.cn
FAU - Jia, Shumin
AU  - Jia S
FAU - Ding, Ning
AU  - Ding N
FAU - Zhao, Wenying
AU  - Zhao W
FAU - Wang, Shujuan
AU  - Wang S
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
EDAT- 2010/04/01 06:00
MHDA- 2010/04/01 06:01
CRDT- 2010/04/01 06:00
PHST- 2010/04/01 06:00 [entrez]
PHST- 2010/04/01 06:00 [pubmed]
PHST- 2010/04/01 06:01 [medline]
PST - ppublish
SO  - Se Pu. 2009 Nov;27(6):849-51.