PMID- 20458925
OWN - NLM
STAT- MEDLINE
DCOM- 20111205
LR  - 20190923
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 28
IP  - 1
DP  - 2010 Jan
TI  - [Determination of 15 volatile organic compound residues in cosmetics by headspace 
      gas chromatography].
PG  - 73-7
AB  - A headspace gas chromatography (HS-GC) method was developed for the rapid 
      determination of multimixture of 15 residual volatile organic compounds in 
      cosmetics. The experimental conditions of HS-GC such as headspace temperature, 
      headspace time and the analytical conditions of GC were optimized. Cosmetic 
      samples were extracted and cleaned-up by headspace at 60 degrees C for 30 min, 
      determined by GC-flame ionization detector (FID) and quantified by external 
      standard method. The 15 poisonous volatile organic compounds were separated 
      efficiently from impurities with high sensitivity and reproducibility. The 
      relative standard deviations (RSDs) were less than 5%, the recoveries were from 
      62.8%-116%, the linear range was 0.002-2.0 mg/L with a good linear correlation 
      coefficient (r > 0.999) and the limits of detection were 0.09-0.68 mg/kg. By 
      means of the above developed HS-GC method, 15 residual volatile organic compounds 
      in cosmetics were detected accurately and simultaneously in a single sample 
      injection. The method is accurate, simple, rapid, and is suitable for the trace 
      analysis of multimixture of residual volatile organic compounds in various 
      cosmetics.
FAU - Xu, Yinghua
AU  - Xu Y
AD  - Center for Disease Control and Prevention of Guangdong Province, Guangzhou 
      510300, China. ying9208@163.com
FAU - Zhu, Binghui
AU  - Zhu B
FAU - Zhong, Xiuhua
AU  - Zhong X
FAU - Li, Shaoxia
AU  - Li S
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Cosmetics)
RN  - 0 (Volatile Organic Compounds)
SB  - IM
MH  - Chromatography, Gas/*methods
MH  - Cosmetics/*chemistry
MH  - Volatile Organic Compounds/*analysis
EDAT- 2010/05/13 06:00
MHDA- 2011/12/13 00:00
CRDT- 2010/05/13 06:00
PHST- 2010/05/13 06:00 [entrez]
PHST- 2010/05/13 06:00 [pubmed]
PHST- 2011/12/13 00:00 [medline]
AID - 10.3724/sp.j.1123.2010.00073 [doi]
PST - ppublish
SO  - Se Pu. 2010 Jan;28(1):73-7. doi: 10.3724/sp.j.1123.2010.00073.