PMID- 20549976
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20120105
LR  - 20190923
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 28
IP  - 3
DP  - 2010 Mar
TI  - [Analysis of diuretics by capillary electrochromatography using 
      poly(1-hexadecene-co-TMPTMA) monolithic column].
PG  - 253-9
AB  - A new method for analyzing diuretics by capillary electrochromatography using 
      poly (1-hexadecene-co-TMPTMA) monolithic column was established. Experimental 
      conditions including the mobile phase, separation voltage, and injection 
      condition were optimized for the analysis. Under optimized experimental 
      conditions, six diuretics were separated within 11.0 min with the limits of 
      detection (LODs) (S/N = 3) in the range of 0.35 - 0.65 microg/mL. The method 
      showed good linearity (R2 > or = 0.990 8) in the range 1.15 and 86.0 microg/mL. 
      The recoveries obtained from the analysis of spiked urine sample were between 
      81.9% and 105% with the relative standard deviations (RSDs) lower than 4.7%. It 
      can be concluded that this new method possessed good repeatability and stability 
      in analyzing diuretics, and was successfully applied to the analysis of real 
      urine samples from volunteers. Therefore, this method could be applied to 
      scanning diuretics in human urine samples.
FAU - Lu, Minghua
AU  - Lu M
AD  - Key Laboratory of Analysis and Detection for Food Safety of Ministry of 
      Education, Analytical and Testing Center, Sport Science Research Center, Fuzhou 
      University, Fuzhou 350002, China.
FAU - Li, Xin
AU  - Li X
FAU - Feng, Qiang
AU  - Feng Q
FAU - Chen, Guonan
AU  - Chen G
FAU - Zhang, Lan
AU  - Zhang L
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
EDAT- 2010/06/17 06:00
MHDA- 2010/06/17 06:01
CRDT- 2010/06/17 06:00
PHST- 2010/06/17 06:00 [entrez]
PHST- 2010/06/17 06:00 [pubmed]
PHST- 2010/06/17 06:01 [medline]
AID - 10.3724/sp.j.1123.2010.00253 [doi]
PST - ppublish
SO  - Se Pu. 2010 Mar;28(3):253-9. doi: 10.3724/sp.j.1123.2010.00253.