PMID- 20712115
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20120105
LR  - 20190923
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 28
IP  - 4
DP  - 2010 Apr
TI  - [Determination of 20 carbamate pesticide residues in food by high performance 
      liquid chromatography-tandem mass spectrometry].
PG  - 348-55
AB  - A new method of determination and conformation for 20 carbamate pesticide 
      residues in food by high performance liquid chromatography-tandem mass 
      spectrometry (HPLC-MS/MS) was developed. The residual carbamate pesticides in 
      food were extracted with acetonitrile, cleaned up with C18 solid phase extraction 
      column or Carb/NH2 solid phase extraction column, and the targets were detected 
      and confirmed by HPLC-MS/MS using external standard method. The recoveries of the 
      20 carbamate pesticides in spiked levels (from 0.005 to 0.025 mg/kg) ranged from 
      51.2% to 125.0% with the relative standard deviations (RSDs) from 1.4% to 19.8%; 
      the concentration range of linearity was 0.005-0.1 mg/kg; the correlation 
      coefficients were 0.991 7-0. 999 6. The method is fast, easy, sensitive and 
      reliable. It also demonstrates that this method can meet the requirements for the 
      simultaneous determination of 20 carbamate pesticide residues in food.
FAU - Zhang, Fan
AU  - Zhang F
AD  - Hunan Academy of Inspection & Quarantine, Technology Center of Hunan Entry-Exit 
      Inspection and Quarantine Bureau, Hunan Key Laboratory of Food Safety Science & 
      Technology, Changsha 410004, China.
FAU - Huang, Zhiqiang
AU  - Huang Z
FAU - Zhang, Ying
AU  - Zhang Y
FAU - Li, Zhonghai
AU  - Li Z
FAU - Wang, Meiling
AU  - Wang M
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
EDAT- 2010/08/18 06:00
MHDA- 2010/08/18 06:01
CRDT- 2010/08/18 06:00
PHST- 2010/08/18 06:00 [entrez]
PHST- 2010/08/18 06:00 [pubmed]
PHST- 2010/08/18 06:01 [medline]
AID - 10.3724/sp.j.1123.2010.00348 [doi]
PST - ppublish
SO  - Se Pu. 2010 Apr;28(4):348-55. doi: 10.3724/sp.j.1123.2010.00348.