PMID- 20712116
OWN - NLM
STAT- MEDLINE
DCOM- 20120105
LR  - 20190923
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 28
IP  - 4
DP  - 2010 Apr
TI  - [Determination of 27 industrial dyes in juice and wine using ultra performance 
      liquid chromatography with electrospray ionization tandem quadrupole mass 
      spectrometry].
PG  - 356-62
AB  - A method for the determination of 27 industrial dyes in juice and wine has been 
      developed using ultra performance liquid chromatography-tandem mass spectrometry 
      (UPLC-MS/ MS). Acetonitrile was used as extraction solvent, and sodium chloride 
      was added to salt out the analytes from the samples. Chromatographic separation 
      was performed on a C18 column with the gradient elution and the mass 
      spectrometric acquisition was carried out under the mode of multiple reaction 
      monitoring (MRM). Twenty-four of the 27 dyes were detected under positive 
      ionization mode using the mobile phase of acetonitrile and water containing 0.1% 
      formic acid. The other 3 dyes were analyzed under negative ionization mode with 
      the mobile phase of acetonitrile and water. As a result, the average recoveries 
      of 27 dyes spiked in juice ranged from 57.0% to 117.7% with the relative standard 
      deviations (RSDs) of 2.4%-17.7%, and the average recoveries of 27 dyes spiked in 
      wine ranged from 40.8% to 109.4% with the RSDs of 1.6%-17.9%. The limits of 
      quantification (LOQs) of 27 dyes spiked in juice were in the range of 0.1-50 
      microg/kg, and 0.2-50 microg/kg for those spiked in wine. This method can be 
      applied to rapid detection of illegally added dyes in soft drinks due to its 
      simplicity and high sensitivity.
FAU - Zhao, Shan
AU  - Zhao S
AD  - Beijing Center for Disease Prevention and Control, Beijing 100013, China.
FAU - Zhang, Jing
AU  - Zhang J
FAU - Yang, Yi
AU  - Yang Y
FAU - Shao, Bing
AU  - Shao B
LA  - chi
PT  - English Abstract
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Coloring Agents)
SB  - IM
MH  - Beverages/*analysis
MH  - Chromatography, High Pressure Liquid/*methods
MH  - Coloring Agents/*analysis
MH  - Food Contamination/analysis
MH  - Spectrometry, Mass, Electrospray Ionization/methods
MH  - Tandem Mass Spectrometry/*methods
MH  - Wine/*analysis
EDAT- 2010/08/18 06:00
MHDA- 2012/01/06 06:00
CRDT- 2010/08/18 06:00
PHST- 2010/08/18 06:00 [entrez]
PHST- 2010/08/18 06:00 [pubmed]
PHST- 2012/01/06 06:00 [medline]
AID - 10.3724/sp.j.1123.2010.00356 [doi]
PST - ppublish
SO  - Se Pu. 2010 Apr;28(4):356-62. doi: 10.3724/sp.j.1123.2010.00356.