PMID- 20812631
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20120105
LR  - 20190923
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 28
IP  - 5
DP  - 2010 May
TI  - [Determination of three polycyclic aromatic hydrocarbons in environmental water 
      samples by disposable fibers of solid-phase microextraction coupled with high 
      performance liquid chromatograph].
PG  - 513-6
AB  - A method was developed for the determination of phenanthrene, fluoranthene and 
      chrysene in environmental water samples using disposable fibers of solid-phase 
      microextraction (SPME) coupled with high performance liquid chromatograph (HPLC). 
      The disposable SPME fibers for the extraction were added into the sample (60 mL) 
      spiked with 20 g/L NaCl. After extracted for 60 min at a stirring speed of 1200 
      r/min, the fibers were collected and immersed in 120 microL methanol for 24 h to 
      desorb the analytes for the HPLC analysis followed. Under the optimized 
      conditions, the respective detection limits were 0. 17 microg/L for phenanthrene 
      and fluoranthene, and 0.08 microg/L for chrysene, and the relative standard 
      deviations (RSDs) were less than 8% (n=6). The method was successfully applied to 
      analyze real environmental water samples with spiked recoveries in the range of 
      80.0%-107%. This method is cost-effective, easy to operate, and overcomes the 
      carry-over problem of the pollutants on the fibers.
FAU - Liu, Zhichao
AU  - Liu Z
AD  - State Key Laboratory of Environmental Chemistry and Ecotoxicology, Research 
      Center for Eco-Environmental Sciences, Chinese Academy of Sciences, Beijing 
      100085, China.
FAU - Hu, Xialin
AU  - Hu X
FAU - Liu, Jingfu
AU  - Liu J
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
EDAT- 2010/09/04 06:00
MHDA- 2010/09/04 06:01
CRDT- 2010/09/04 06:00
PHST- 2010/09/04 06:00 [entrez]
PHST- 2010/09/04 06:00 [pubmed]
PHST- 2010/09/04 06:01 [medline]
AID - 10.3724/sp.j.1123.2010.00513 [doi]
PST - ppublish
SO  - Se Pu. 2010 May;28(5):513-6. doi: 10.3724/sp.j.1123.2010.00513.