PMID- 20945062 OWN - NLM STAT- MEDLINE DCOM- 20110131 LR - 20190107 IS - 1432-0800 (Electronic) IS - 0007-4861 (Linking) VI - 86 IP - 1 DP - 2011 Jan TI - Dissipation of oxaziclomefone and residue analysis in rice, soil and water under field conditions. PG - 28-32 LID - 10.1007/s00128-010-0115-9 [doi] AB - The analytical method for the residue analysis of a novel herbicide, oxaziclomefone, and its dissipation in soil, water, rice plants and husked rice in rice fields at GAP (Good Agricultural Practices) conditions were studied. Oxaziclomefone residues were determined by GC-NPD. Mean recoveries ranged from 84.4 to 108.2% with relative standard deviations (RSDs) of 2.4 to 17.2% at three different spiking levels for each different matrix. The limits of quantification (LOQ) were found to be 0.01 mg/kg in soil, water, rice plants and husked rice and 0.02 mg/kg in rice hull. The mean half-lives of oxaziclomefone residues in water, soil and rice plants were 11.3, 37 and 4.4 days, respectively. At harvest, soil, straw, rice hull and husked rice samples were found to contain oxaziclomefone below the maximum residue level (0.1 mg/kg) set by Japan and Korea. Following the recommended application method, this herbicide is therefore safe to apply to rice fields. FAU - Liang, Hongwu AU - Liang H AD - College of Science, China Agricultural University, 100193 Beijing, People's Republic of China. FAU - Li, Li AU - Li L FAU - Ji, Ran AU - Ji R FAU - Qin, Dongmei AU - Qin D FAU - Liu, Fengmao AU - Liu F LA - eng PT - Journal Article PT - Research Support, Non-U.S. Gov't DEP - 20101014 PL - United States TA - Bull Environ Contam Toxicol JT - Bulletin of environmental contamination and toxicology JID - 0046021 RN - 0 (Environmental Pollutants) RN - 0 (Herbicides) RN - 0 (Oxazines) RN - 0 (Pesticide Residues) RN - 0 (Soil) RN - 6O05VST8NA (oxaziclomefone) SB - IM MH - Environmental Monitoring/methods MH - Environmental Pollutants/*analysis/chemistry MH - Fresh Water/chemistry MH - Half-Life MH - Herbicides/*analysis/chemistry MH - Oryza/*chemistry MH - Oxazines/*analysis/chemistry MH - Pesticide Residues/*analysis/chemistry MH - Soil/chemistry EDAT- 2010/10/15 06:00 MHDA- 2011/02/01 06:00 CRDT- 2010/10/15 06:00 PHST- 2010/06/04 00:00 [received] PHST- 2010/09/27 00:00 [accepted] PHST- 2010/10/15 06:00 [entrez] PHST- 2010/10/15 06:00 [pubmed] PHST- 2011/02/01 06:00 [medline] AID - 10.1007/s00128-010-0115-9 [doi] PST - ppublish SO - Bull Environ Contam Toxicol. 2011 Jan;86(1):28-32. doi: 10.1007/s00128-010-0115-9. Epub 2010 Oct 14.