PMID- 21131243
OWN - NLM
STAT- MEDLINE
DCOM- 20110411
LR  - 20131121
IS  - 1873-376X (Electronic)
IS  - 1570-0232 (Linking)
VI  - 879
IP  - 1
DP  - 2011 Jan 1
TI  - Determination of neonicotinoid insecticides residues in bovine tissues by 
      pressurized solvent extraction and liquid chromatography-tandem mass 
      spectrometry.
PG  - 117-22
LID - 10.1016/j.jchromb.2010.11.008 [doi]
AB  - A rapid, sensitive, and environmental-friendly method has been developed for the 
      simultaneous determination of seven neonicotinoid insecticides residues in bovine 
      muscle and liver. The sample preparation procedure was based on a high automated 
      pressurized solvent extraction (PSE) combined with solid-phase extraction (SPE) 
      clean-up. The target compounds were identified and quantitatively determined by 
      liquid chromatography coupled with electrospray ionization tandem mass 
      spectrometry (LC-ESI-MS/MS) operated in multiple reaction monitoring mode. 
      Average recoveries of the seven analytes from fortified samples ranged between 
      83.2% and 101.9%, with relative standard deviations (RSDs) lower than 10.8%. The 
      limits of detection (LODs) and quantification (LOQs) for neonicotinoids were in 
      the ranges of 0.8-1.5 mugkg(-)(1) and 2.5-5.0 mugkg(-)(1), respectively. This validated 
      method was successively applied to the determination of neonicotinoid 
      insecticides in real samples from markets.
CI  - Copyright (c) 2010 Elsevier B.V. All rights reserved.
FAU - Xiao, Zhiming
AU  - Xiao Z
AD  - Department of Pharmacology and Toxicology, College of Veterinary Medicine, China 
      Agricultural University, Beijing 100193, China.
FAU - Li, Xiaowei
AU  - Li X
FAU - Wang, Xiaolin
AU  - Wang X
FAU - Shen, Jianzhong
AU  - Shen J
FAU - Ding, Shuangyang
AU  - Ding S
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
DEP - 20101119
PL  - Netherlands
TA  - J Chromatogr B Analyt Technol Biomed Life Sci
JT  - Journal of chromatography. B, Analytical technologies in the biomedical and life 
      sciences
JID - 101139554
RN  - 0 (Insecticides)
RN  - 0 (Pesticide Residues)
RN  - LMS11II2LO (Anabasine)
SB  - IM
MH  - Anabasine/*analysis/chemistry
MH  - Animals
MH  - Cattle
MH  - Chemical Fractionation/*methods
MH  - Chromatography, Liquid/*methods
MH  - Insecticides/*analysis/chemistry
MH  - Liver/chemistry
MH  - Muscles/chemistry
MH  - Pesticide Residues/*analysis/chemistry
MH  - Reproducibility of Results
MH  - Sensitivity and Specificity
MH  - Tandem Mass Spectrometry/*methods
EDAT- 2010/12/07 06:00
MHDA- 2011/04/13 06:00
CRDT- 2010/12/07 06:00
PHST- 2010/09/11 00:00 [received]
PHST- 2010/11/02 00:00 [revised]
PHST- 2010/11/04 00:00 [accepted]
PHST- 2010/12/07 06:00 [entrez]
PHST- 2010/12/07 06:00 [pubmed]
PHST- 2011/04/13 06:00 [medline]
AID - S1570-0232(10)00690-2 [pii]
AID - 10.1016/j.jchromb.2010.11.008 [doi]
PST - ppublish
SO  - J Chromatogr B Analyt Technol Biomed Life Sci. 2011 Jan 1;879(1):117-22. doi: 
      10.1016/j.jchromb.2010.11.008. Epub 2010 Nov 19.