PMID- 21261051
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20120213
LR  - 20190923
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 28
IP  - 8
DP  - 2010 Aug
TI  - [Determination of 10 volatile organic compounds in toys by headspace gas 
      chromatography-mass spectrometry].
PG  - 800-4
AB  - A headspace gas chromatography-mass spectrometry (HS-GC-MS) method was developed 
      for the determination of 10 residual volatile organic compounds (VOCs) in toys. 
      The experimental conditions such as headspace temperature, headspace time and the 
      analytical conditions of GC-MS were optimized. Toy samples were treated at 140 
      degrees C for 45 min, and then the evolved products were separated on a DB-624 
      column, determined by MS and quantified by external standard method. The 
      recoveries were from 79% to 106% and the relative standard deviations (RSDs) were 
      from 0.4% to 5.6%. The linear range was 0.001 - 2.0 microg with a good linear 
      correlation coefficient (r > 0.994 0) and the limits of quantification (LOQ) were 
      less than 0 66 mg/kg. The method is accurate, simple, rapid, and is suitable for 
      the analysis of residual VOCs in various toys.
FAU - Lu, Qing
AU  - Lu Q
AD  - Institute of Industrial Product Inspection, Chinese Academy of Inspection and 
      Quarantine, Beijing 100123, China.
FAU - Zhang, Qing
AU  - Zhang Q
FAU - Kang, Suyuan
AU  - Kang S
FAU - Bai, Hua
AU  - Bai H
FAU - Wang, Chao
AU  - Wang C
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
EDAT- 2011/01/26 06:00
MHDA- 2011/01/26 06:01
CRDT- 2011/01/26 06:00
PHST- 2011/01/26 06:00 [entrez]
PHST- 2011/01/26 06:00 [pubmed]
PHST- 2011/01/26 06:01 [medline]
AID - 10.3724/sp.j.1123.2010.00800 [doi]
PST - ppublish
SO  - Se Pu. 2010 Aug;28(8):800-4. doi: 10.3724/sp.j.1123.2010.00800.