PMID- 21381430
OWN - NLM
STAT- MEDLINE
DCOM- 20120213
LR  - 20161018
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 28
IP  - 11
DP  - 2010 Nov
TI  - [Determination of histamine in canned fish by high performance liquid 
      chromatography with pre-column derivatization].
PG  - 1099-102
AB  - A pre-column derivatization-high performance liquid chromatographic (HPLC) method 
      has been developed for the determination of histamine in canned fish. The 
      homogenated samples were ultrasonically extracted with perchloric acid aqueous 
      solution, derivatized with dansyl chloride and diluted with acetonitrile to a 
      desired volume. The samples were determined by HPLC with ultraviolet detector and 
      quantified by external standard method. Adopting a C18 column with 1.8 microm 
      stationary phase particles, the analysis time for each sample was smaller than 5 
      min with the flow rate of 0.3 mL/min. It can decrease the consumption of the 
      mobile phase and save the cost. The linear range was 0.08-8.00 mg/L for 
      histamine. The correlation coefficient was 0.999 98. The average recoveries of 
      histamine at different concentration levels in spiked samples were greater than 
      96% and the relative standard deviations (RSDs) were smaller than 2.5%. The 
      quantitation limit was 5.00 mg/kg for histamine in canned fish by HPLC. The 
      results indicated that this HPLC method is fast, sensitive, reproducible and 
      practical for the routine analysis of histamine in canned fish.
FAU - Jin, Gaowa
AU  - Jin G
AD  - East China Sea Fishery Research Institute, Chinese Academy of Fishery Sciences, 
      Fishery Products Quality Inspection and Test Center (Shanghai), Ministry of 
      Agriculture of China, Shanghai 200090, China. jgw200406@126.com
FAU - Cai, Youqiong
AU  - Cai Y
FAU - Yu, Huijuan
AU  - Yu H
FAU - Qian, Beilei
AU  - Qian B
LA  - chi
PT  - English Abstract
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 820484N8I3 (Histamine)
SB  - IM
MH  - Animals
MH  - Chromatography, High Pressure Liquid/*methods
MH  - Fish Products/*analysis
MH  - Food Contamination/*analysis
MH  - Food, Preserved/*analysis
MH  - Histamine/*analysis
EDAT- 2011/03/09 06:00
MHDA- 2012/02/14 06:00
CRDT- 2011/03/09 06:00
PHST- 2011/03/09 06:00 [entrez]
PHST- 2011/03/09 06:00 [pubmed]
PHST- 2012/02/14 06:00 [medline]
PST - ppublish
SO  - Se Pu. 2010 Nov;28(11):1099-102.