PMID- 21381431
OWN - NLM
STAT- MEDLINE
DCOM- 20120213
LR  - 20171116
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 28
IP  - 11
DP  - 2010 Nov
TI  - [Determination of nitenpyram residue in cabbage and soil using gas 
      chromatography].
PG  - 1103-6
AB  - An analytical method for the determination of nitenpyram residue in cabbage and 
      soil using gas chromatography was established. The nitenpyram residue was 
      extracted from cabbage and soil with acetone-water (4 : 1, v/v), cleaned up by a 
      Florisil column, and then detected by gas chromatography-electron capture 
      detection (GC-ECD). At the spiked level range from 0.02 to 2.00 mg/kg, the 
      average recoveries of nitenpyram were 88.73%-94.3% and 90.82%-96.27% with the 
      relative standard deviations (RSDs) of 3.09%-7.39% and 2.01%-4.92% in cabbage and 
      soil, respectively. The limit of detection of nitenpyram was 0.02 mg/kg. The 
      method is fast, sensitive, simple, reproducible and practical for the 
      determination of nitenpyram residue in environmental systems.
FAU - Zhang, Guiqun
AU  - Zhang G
AD  - College of Agriculture, Guangxi University, Nanning 530004, China.
FAU - Nie, Siqiao
AU  - Nie S
FAU - Long, Liping
AU  - Long L
FAU - Zeng, Dongqiang
AU  - Zeng D
FAU - Chen, Jiuxing
AU  - Chen J
FAU - Yang, Hui
AU  - Yang H
FAU - Chen, Linglong
AU  - Chen L
LA  - chi
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Insecticides)
RN  - 0 (Neonicotinoids)
RN  - 0 (Pesticide Residues)
RN  - 0 (Pyridines)
RN  - 0 (Soil)
RN  - 0 (Soil Pollutants)
RN  - 3A837VZ81Y (nitenpyram)
SB  - IM
MH  - Brassica/*chemistry
MH  - Chromatography, Gas/*methods
MH  - Insecticides/analysis
MH  - Neonicotinoids
MH  - Pesticide Residues/*analysis
MH  - Pyridines/*analysis
MH  - Soil/analysis
MH  - Soil Pollutants/*analysis
EDAT- 2011/03/09 06:00
MHDA- 2012/02/14 06:00
CRDT- 2011/03/09 06:00
PHST- 2011/03/09 06:00 [entrez]
PHST- 2011/03/09 06:00 [pubmed]
PHST- 2012/02/14 06:00 [medline]
PST - ppublish
SO  - Se Pu. 2010 Nov;28(11):1103-6.