PMID- 21574398
OWN - NLM
STAT- MEDLINE
DCOM- 20120628
LR  - 20190923
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 29
IP  - 1
DP  - 2011 Jan
TI  - [Determination of 46 plasticizers in food contact polyvinyl chloride packaging 
      materials and their migration into food simulants by gas chromatography-mass 
      spectrometry].
PG  - 42-8
AB  - A gas chromatography-mass spectrometry (GC-MS) method was developed for the 
      determination of 46 plasticizers in food contact polyvinyl chloride (PVC) 
      packaging materials and their migration into food simulants, i. e. water, 3% 
      acetic acid, 10% ethanol and olive oil. Plasticizers in the PVC packaging 
      materials, aqueous food simulants and olive oil food simulants were extracted by 
      the dissolution-precipitation, liquid-liquid extraction and gel permeation 
      chromatography (GPC) approaches, respectively. The extracts were analyzed by 
      GC-MS in selective ion monitoring (SIM) mode and quantified using the external 
      standard method. The cal-ibration curves were linear in the ranges of 0.1-2.0 
      mg/L with the correlation coefficients of 0.9910-0. 999 9. The limits of 
      detection were from 0. 005 mg/kg to 0. 05 mg/kg ( S/N = 5 ). The recoveries at 3 
      spiked levels were 69.51%-107. 21% and the relative standard deviations (RSDs n = 
      6) ranged from 3.53% to 18.95%. These results show that this method is fast, 
      sensitive and accurate for the qualitative and quantitative determination of 
      plasticizers in food contact plastic products and 4 types of food simulants.
FAU - Guo, Chunhai
AU  - Guo C
AD  - Hebei Entry-Exit Inspection and Quarantine Bureau, Shjiazhuang 050051, China.
FAU - Bo, Haibo
AU  - Bo H
FAU - Duan, Wenzhong
AU  - Duan W
FAU - Jia, Haitao
AU  - Jia H
FAU - Chen, Ruichun
AU  - Chen R
FAU - Ma, Yusong
AU  - Ma Y
FAU - Ai, Lianfeng
AU  - Ai L
LA  - chi
PT  - English Abstract
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Plasticizers)
RN  - 9002-86-2 (Polyvinyl Chloride)
SB  - IM
MH  - Food Contamination/*analysis
MH  - *Food Packaging/methods
MH  - Gas Chromatography-Mass Spectrometry/*methods
MH  - Plasticizers/*analysis
MH  - Polyvinyl Chloride/*chemistry
EDAT- 2011/05/18 06:00
MHDA- 2012/06/29 06:00
CRDT- 2011/05/18 06:00
PHST- 2011/05/18 06:00 [entrez]
PHST- 2011/05/18 06:00 [pubmed]
PHST- 2012/06/29 06:00 [medline]
AID - 10.3724/sp.j.1123.2011.00042 [doi]
PST - ppublish
SO  - Se Pu. 2011 Jan;29(1):42-8. doi: 10.3724/sp.j.1123.2011.00042.