PMID- 21847972
OWN - NLM
STAT- MEDLINE
DCOM- 20120802
LR  - 20190923
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 29
IP  - 5
DP  - 2011 May
TI  - [Determination of bisphenol A in milk by liquid chromatography-tandem mass 
      spectrometry coupled with solid phase extraction of monodisperse magnetic 
      submicron particles as adsorbent].
PG  - 399-403
AB  - Monodisperse magnetic submicron particles were synthesized by a solvothermal 
      reduction method. A solid phase extraction (SPE) based on the monodisperse 
      magnetic submicron particles and high performance liquid chromatography-tandem 
      mass spectrometry (HPLC-MS/MS) method for the determination of bisphenol A (BPA) 
      at trace level in milk has been established. The important parameters that affect 
      the extraction efficiency such as the solution pH, dosage of magnetic submicron 
      particles, nature of elution solution and its volume were optimized. The optimal 
      extraction conditions were as follows: the pH 6.0, the dosage of 3.5 mg magnetic 
      submicron particles and 0.4 mL methanol as elution solution. BPA was analyzed by 
      HPLC-MS/MS in negative ion mode using an Agilent XDB C18 column as analytical 
      column. Under the optimal conditions, the calibration curves showed a good 
      linearity in the BPA concentration range of 1.0-100.0 micro g/L. The correlation 
      coefficient was 0. 999 3. The average recoveries of BPA at three spiked levels 
      ranged from 85.3% to 96. 1% with the relative standard deviations (RSDs) less 
      than 10%. The detection limit of the method was 1.0 microg/L. The method is 
      sensitive, simple, and suitable for the rapid determination of BPA in milk.
FAU - Wu, Xinhua
AU  - Wu X
AD  - Faculty of Food Science & Engineering, Central South University of Forestry & 
      Technology, Changsha 410004, China.
FAU - Ding, Li
AU  - Ding L
FAU - Xiao, Jiayong
AU  - Xiao J
FAU - Long, Yanjiao
AU  - Long Y
FAU - Xu, Zhou
AU  - Xu Z
FAU - Li, Zhonghai
AU  - Li Z
FAU - Wang, Libing
AU  - Wang L
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Benzhydryl Compounds)
RN  - 0 (Phenols)
RN  - MLT3645I99 (bisphenol A)
RN  - XM0M87F357 (Ferrosoferric Oxide)
SB  - IM
MH  - Animals
MH  - Benzhydryl Compounds
MH  - Chromatography, Liquid/*methods
MH  - Ferrosoferric Oxide/chemistry
MH  - Food Contamination/*analysis
MH  - Milk/*chemistry
MH  - Particle Size
MH  - Phenols/*analysis
MH  - Solid Phase Extraction/methods
MH  - Tandem Mass Spectrometry/*methods
EDAT- 2011/08/19 06:00
MHDA- 2012/08/03 06:00
CRDT- 2011/08/19 06:00
PHST- 2011/08/19 06:00 [entrez]
PHST- 2011/08/19 06:00 [pubmed]
PHST- 2012/08/03 06:00 [medline]
AID - 10.3724/sp.j.1123.2011.00399 [doi]
PST - ppublish
SO  - Se Pu. 2011 May;29(5):399-403. doi: 10.3724/sp.j.1123.2011.00399.