PMID- 21959994
OWN - NLM
STAT- MEDLINE
DCOM- 20120322
LR  - 20171116
IS  - 1432-0800 (Electronic)
IS  - 0007-4861 (Linking)
VI  - 87
IP  - 6
DP  - 2011 Dec
TI  - Determination of hymexazol in cucumber and soil samples by derivatization using 
      GC-FPD.
PG  - 653-6
LID - 10.1007/s00128-011-0421-x [doi]
AB  - A sensitive and effective analytical method for the determination of hymexazol in 
      cucumber and soil samples by gas chromatography with a flame photometric detector 
      was developed. This method was validated with fortified at three different levels 
      of 0.2, 1.0 and 5.0 mg/kg. Average recoveries obtained from cucumber and soil 
      samples at three fortified levels were 94.0%-107.8% with relative standard 
      deviations (RSDs) of less than 11.4%. Limits of quantification (LOQ) in cucumber 
      and soil were 0.2 mg/kg. The method was successfully applied to determine 
      hymexazol in real samples of cucumber and soil under open fields.
FAU - Sun, Dali
AU  - Sun D
AD  - Key Laboratory of Natural Pesticide and Chemical Biology, Ministry of Education, 
      South China Agricultural University, Guangzhou, 510642, People's Republic of 
      China.
FAU - Li, Li
AU  - Li L
FAU - Ji, Ran
AU  - Ji R
FAU - Li, Wei
AU  - Li W
FAU - Ye, Huochun
AU  - Ye H
FAU - Wu, Yijun
AU  - Wu Y
FAU - Liu, Chenglan
AU  - Liu C
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
DEP - 20110930
PL  - United States
TA  - Bull Environ Contam Toxicol
JT  - Bulletin of environmental contamination and toxicology
JID - 0046021
RN  - 0 (Oxazoles)
RN  - 0 (Pesticide Residues)
RN  - 0 (Soil)
RN  - 0 (Soil Pollutants)
RN  - 20T2M875LO (hymexazol)
SB  - IM
MH  - Chromatography, Gas/*methods
MH  - Cucumis sativus/*chemistry
MH  - Environmental Monitoring/*methods
MH  - Guidelines as Topic
MH  - Oxazoles/*analysis
MH  - Pesticide Residues/analysis
MH  - Soil/analysis/*chemistry
MH  - Soil Pollutants/*analysis
EDAT- 2011/10/01 06:00
MHDA- 2012/03/23 06:00
CRDT- 2011/10/01 06:00
PHST- 2011/06/01 00:00 [received]
PHST- 2011/09/19 00:00 [accepted]
PHST- 2011/10/01 06:00 [entrez]
PHST- 2011/10/01 06:00 [pubmed]
PHST- 2012/03/23 06:00 [medline]
AID - 10.1007/s00128-011-0421-x [doi]
PST - ppublish
SO  - Bull Environ Contam Toxicol. 2011 Dec;87(6):653-6. doi: 
      10.1007/s00128-011-0421-x. Epub 2011 Sep 30.