PMID- 22032170
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20120802
LR  - 20190923
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 29
IP  - 6
DP  - 2011 Jun
TI  - [Determination of phthalic acid esters in soil by gas chromatography-tandem mass 
      spectrometry].
PG  - 563-6
AB  - A method based on gas chromatography-tandem mass spectrometry (GC-MS/MS) was 
      developed for the determination of phthalic acid esters (PAEs) in soil. The soil 
      sample was extracted by dichloromethane-acetone (1: 1, v/v) with an ultrasonic 
      instrument, and the extract was cleaned up with a Florisil column. The 
      identification and quantification of the analytes were carried out in the 
      multiple reaction monitoring (MRM) mode after the GC separation on an HP-5MS 
      column (30 m x 0.25 mm x 0.25 microm). The eight point calibration curves showed 
      a good linearity for all the congeners (0.997 3 - 0.997 6). The limits of 
      detection (LODs) ranged from 0.1 to 0.5 microg/kg. The relative standard 
      deviations (RSDs) were not more than 14.3% and the spiked recoveries were in the 
      range of 72.9% - 106.2%. The developed analytical method is rapid and accurate, 
      and suitable for the determination of PAEs in soil.
FAU - Li, Hong
AU  - Li H
AD  - Liaoning Province Academy of Analytic Sciences, Standard System Engineering 
      Research Center of Liaoning Province, Shenyang 110015, China. lh_9214@163.com
FAU - Tian, Fulin
AU  - Tian F
FAU - Ren, Xuedong
AU  - Ren X
FAU - Wang, Xinrui
AU  - Wang X
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
EDAT- 2011/10/29 06:00
MHDA- 2011/10/29 06:01
CRDT- 2011/10/29 06:00
PHST- 2011/10/29 06:00 [entrez]
PHST- 2011/10/29 06:00 [pubmed]
PHST- 2011/10/29 06:01 [medline]
AID - 10.3724/sp.j.1123.2011.00563 [doi]
PST - ppublish
SO  - Se Pu. 2011 Jun;29(6):563-6. doi: 10.3724/sp.j.1123.2011.00563.