PMID- 22268362
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20121015
LR  - 20161018
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 29
IP  - 10
DP  - 2011 Oct
TI  - [Determination of three polycyclic aromatic hydrocarbons in mainstream cigarette 
      smoke by automated solid phase extraction system-gas chromatography-tandem mass 
      spectrometry].
PG  - 1031-5
AB  - A simple method for the analysis of benzo [ a ] pyrene, benzo [ a ] anthracene 
      and chrysene in mainstream cigarette smoke using automated solid phase extraction 
      (SPE) system-gas chromatography-tandem mass spectrometry (GC-MS/MS) was 
      developed. After being smoked in the ISO mode, the Cambridge filter pad was used 
      to collect mainstream cigarette smoke, and then extracted by 40 mL cyclohexane 
      containing deuterated benzo [a] pyrene as the internal standard. The extract was 
      cleaned-up by an automated PrepLinc SPE-AccuVap system and then detected using 
      GC-MS/MS. The detection limits for benzo [a] pyrene, benzo [a] anthracene and 
      chrysene were 0.05,0. 16, and 0.23 ng/cig, respectively. The recoveries were 
      ranged from 91.5% to 102.1% to 102.1% with the relative standard deviations 
      (RSDs) less than 5%. This method was proved to be simple, sensitive, and suitable 
      for the determination of benzo [a] pyrene, benzo[a] anthracene and chrysene in 
      mainstream cigarette smoke.
FAU - Bian, Zhaoyang
AU  - Bian Z
AD  - China National Tobacco Quality Supervision & Test Center, Zhengzhou 450001, 
      China.
FAU - Tang, Gangling
AU  - Tang G
FAU - Chen, Zaigen
AU  - Chen Z
FAU - Pang, Yongqiang
AU  - Pang Y
FAU - Jiang, Xingyi
AU  - Jiang X
FAU - Hu, Qingyuian
AU  - Hu Q
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
EDAT- 2012/01/25 06:00
MHDA- 2012/01/25 06:01
CRDT- 2012/01/25 06:00
PHST- 2012/01/25 06:00 [entrez]
PHST- 2012/01/25 06:00 [pubmed]
PHST- 2012/01/25 06:01 [medline]
PST - ppublish
SO  - Se Pu. 2011 Oct;29(10):1031-5.