PMID- 23016299
OWN - NLM
STAT- MEDLINE
DCOM- 20130809
LR  - 20190923
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 30
IP  - 6
DP  - 2012 Jun
TI  - [Simultaneous determination of seven naphthalenediols in cosmetics by 
      reversed-phase high performance liquid chromatography].
PG  - 630-4
AB  - A novel analytical method for the simultaneous determination of seven 
      naphthalenediols (2,6-naphthalenediol, 1,5-naphthalenediol, 1,6-naphthalenediol, 
      2,7-naphthalenediol, 1,7-naphthalenediol, 1,3-naphthalenediol and 
      2,3-naphthalenediol) in cosmetics by reversed-phase high performance liquid 
      chromatography (RP-HPLC) with a diode array detector was established. The 
      moisturizer, cream, emulsion and water-like cosmetic samples were extracted with 
      95% ethanol (v/v), and the powder-like cosmetic samples were extracted with 95% 
      ethanol-0.1% acetic acid (3: 2, v/v), then the extracts were centrifuged, 
      filtrated, and analyzed by RP-HPLC using a C18 column, employing methanol-0.1% 
      acetic acid aqueous solution as the mobile phases under the condition of gradient 
      elution. The naphthalenediols were qualitatively determined by retention times, 
      and confirmed by ultraviolet spectra. The external standard method was applied 
      for the quantification. The results indicated that the limits of quantification 
      (LOQs) of the seven naphthalenediols were ranged from 0.5 mg/kg to 1.2 mg/kg (S/N 
      = 10); meanwhile, the linear correlation coefficients of them were all no less 
      than 0.999 0 within the linear ranges. Their recoveries in spiked samples at the 
      levels of 5.0 - 50 mg/kg were ranged from 84.0% to 102% with the relative 
      standard deviations (RSDs) of 1.3% - 5.7% (n = 6). The method is simple, precise 
      and suitable for the determination of naphthalenediols in cosmetic samples.
FAU - Chen, Lijian
AU  - Chen L
AD  - Guangzhou Quality Supervision and Testing Institute, Guangzhou 510110, China.
FAU - Huang, Jinfeng
AU  - Huang J
FAU - He, Minheng
AU  - He M
FAU - Lin, Senyu
AU  - Lin S
FAU - Guo, Xindong
AU  - Guo X
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Cosmetics)
RN  - 0 (Naphthols)
SB  - IM
MH  - Chromatography, High Pressure Liquid/*methods
MH  - Chromatography, Reverse-Phase/*methods
MH  - Cosmetics/*analysis/chemistry
MH  - Naphthols/*analysis/chemistry
EDAT- 2012/09/29 06:00
MHDA- 2013/08/10 06:00
CRDT- 2012/09/29 06:00
PHST- 2012/09/29 06:00 [entrez]
PHST- 2012/09/29 06:00 [pubmed]
PHST- 2013/08/10 06:00 [medline]
AID - 10.3724/sp.j.1123.2012.02015 [doi]
PST - ppublish
SO  - Se Pu. 2012 Jun;30(6):630-4. doi: 10.3724/sp.j.1123.2012.02015.